One-pot synthesis of new 6-(alkylamine)dibenzo[c,e][1,2]oxaphosphinine-6-oxides
José Gustavo Ávila Zárraga
1
,
Ignacio Pérez
1
,
Erick Beristain
1
,
Irma Gavilan
1
,
Moisés Romero
2
2
Facultad de Química, Universidad del Estado de México, PaseoColón/Paseo Tollocan, Mexico
|
Publication type: Journal Article
Publication date: 2017-01-19
scimago Q3
wos Q3
SJR: 0.322
CiteScore: 4.3
Impact factor: 1.8
ISSN: 00397911, 15322432
Organic Chemistry
Abstract
ABSTRACTSeveral new 6-(alkylamine)-6H-dibenz[c,e][1,2]oxaphosphinine-6-oxides were prepared through a one-pot reaction, starting with 2-phenylphenol, phosphorus trichloride, and a Zn catalyst, to form 6-chloro-6H-dibenz[c,e][1,2]oxaphosphine. The alkylamine derivatives were subsequently prepared through a nucleophilic substitution reaction involving aliphatic amines and H2O2 oxidation under soft conditions. This method has the advantages that it is a one-pot synthesis, does not require an inert atmosphere, and involves in situ catalyst formation.
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Ávila Zárraga J. G. et al. One-pot synthesis of new 6-(alkylamine)dibenzo[c,e][1,2]oxaphosphinine-6-oxides // Synthetic Communications. 2017. Vol. 47. No. 4. pp. 364-367.
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Ávila Zárraga J. G., Pérez I., Beristain E., Gavilan I., Romero M. One-pot synthesis of new 6-(alkylamine)dibenzo[c,e][1,2]oxaphosphinine-6-oxides // Synthetic Communications. 2017. Vol. 47. No. 4. pp. 364-367.
Cite this
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TY - JOUR
DO - 10.1080/00397911.2016.1265651
UR - https://doi.org/10.1080/00397911.2016.1265651
TI - One-pot synthesis of new 6-(alkylamine)dibenzo[c,e][1,2]oxaphosphinine-6-oxides
T2 - Synthetic Communications
AU - Ávila Zárraga, José Gustavo
AU - Pérez, Ignacio
AU - Beristain, Erick
AU - Gavilan, Irma
AU - Romero, Moisés
PY - 2017
DA - 2017/01/19
PB - Taylor & Francis
SP - 364-367
IS - 4
VL - 47
SN - 0039-7911
SN - 1532-2432
ER -
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BibTex (up to 50 authors)
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@article{2017_Ávila Zárraga,
author = {José Gustavo Ávila Zárraga and Ignacio Pérez and Erick Beristain and Irma Gavilan and Moisés Romero},
title = {One-pot synthesis of new 6-(alkylamine)dibenzo[c,e][1,2]oxaphosphinine-6-oxides},
journal = {Synthetic Communications},
year = {2017},
volume = {47},
publisher = {Taylor & Francis},
month = {jan},
url = {https://doi.org/10.1080/00397911.2016.1265651},
number = {4},
pages = {364--367},
doi = {10.1080/00397911.2016.1265651}
}
Cite this
MLA
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Ávila Zárraga, José Gustavo, et al. “One-pot synthesis of new 6-(alkylamine)dibenzo[c,e][1,2]oxaphosphinine-6-oxides.” Synthetic Communications, vol. 47, no. 4, Jan. 2017, pp. 364-367. https://doi.org/10.1080/00397911.2016.1265651.