Synthetic Communications

, том 21 , издание 8-9 , страницы 1075-1081

An Improved and Simple Synthesis of Methyl or Ethyl 7-Oxoheptanoate and 7-Acetoxyheptanal

Тип публикации: Journal Article

Дата публикации: 1991-04-01

Taylor & Francis

Synthetic Communications

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SJR: 0.322

CiteScore: 4.3

Impact factor: 1.8

ISSN: 00397911, 15322432

DOI: 10.1080/00397919108019797

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Organic Chemistry

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Reaction of cycloheptanone with potassium persulfate, in ethanol or methanol, gave ethyl or methyl 7-hydroxyheptanoate which, by oxidation with PCC, were converted into ethyl or methyl 7-oxoheptanoate in good yields. Protection of aldehyde group of methyl 7-oxoheptanoate, followed by one-step conversion of carboxylic ester to the acetate gave, after regeneration of aldehyde group, 7-acetoxyheptanal.

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Ballini R., Marcantoni E., Petrini M. An Improved and Simple Synthesis of Methyl or Ethyl 7-Oxoheptanoate and 7-Acetoxyheptanal // Synthetic Communications. 1991. Vol. 21. No. 8-9. pp. 1075-1081.

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Ballini R., Marcantoni E., Petrini M. An Improved and Simple Synthesis of Methyl or Ethyl 7-Oxoheptanoate and 7-Acetoxyheptanal // Synthetic Communications. 1991. Vol. 21. No. 8-9. pp. 1075-1081.

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TY - JOUR

DO - 10.1080/00397919108019797

UR - https://doi.org/10.1080/00397919108019797

TI - An Improved and Simple Synthesis of Methyl or Ethyl 7-Oxoheptanoate and 7-Acetoxyheptanal

T2 - Synthetic Communications

AU - Ballini, Roberto

AU - Marcantoni, Enrico

AU - Petrini, Marino

PY - 1991

DA - 1991/04/01

PB - Taylor & Francis

SP - 1075-1081

IS - 8-9

VL - 21

SN - 0039-7911

SN - 1532-2432

ER -

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@article{1991_Ballini,

author = {Roberto Ballini and Enrico Marcantoni and Marino Petrini},

title = {An Improved and Simple Synthesis of Methyl or Ethyl 7-Oxoheptanoate and 7-Acetoxyheptanal},

journal = {Synthetic Communications},

year = {1991},

volume = {21},

publisher = {Taylor & Francis},

month = {apr},

url = {https://doi.org/10.1080/00397919108019797},

number = {8-9},

pages = {1075--1081},

doi = {10.1080/00397919108019797}

}

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Ballini, Roberto, et al. “An Improved and Simple Synthesis of Methyl or Ethyl 7-Oxoheptanoate and 7-Acetoxyheptanal.” Synthetic Communications, vol. 21, no. 8-9, Apr. 1991, pp. 1075-1081. https://doi.org/10.1080/00397919108019797.