The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction
Тип публикации: Journal Article
Дата публикации: 2018-04-13
scimago Q3
wos Q4
БС3
SJR: 0.201
CiteScore: 1.3
Impact factor: 0.7
ISSN: 15421406, 15635287, 00268941, 10568816
General Chemistry
Condensed Matter Physics
General Materials Science
Краткое описание
Abstract Crystals of bis-chloromethyl-phosphinic acid ((CH2Cl)2POOH) are studied by attenuated total reflection (ATR) and Raman spectroscopy supported by X-Ray diffraction. The bands recorded in the ATR and in Raman spectra have the same wavenumbers within experimental uncertainty. It is in agreement with the X-Ray diffraction results which show that the molecules in crystals form infinite chains through hydrogen bonds and there is no center of inversion. The parameters of the unit cell, the bond lengths and angles, and the distance between two oxygen atoms in hydrogen bond bridges are determined. The spectral features and the intermolecular distance between oxygen atoms are characteristic for a strong hydrogen bonded system.
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Journal of Molecular Structure
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Glazachev E. V., Avdontceva M. S., Asfin R. E. The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction // Molecular Crystals and Liquid Crystals. 2018. Vol. 665. No. 1. pp. 219-227.
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Glazachev E. V., Avdontceva M. S., Asfin R. E. The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction // Molecular Crystals and Liquid Crystals. 2018. Vol. 665. No. 1. pp. 219-227.
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TY - JOUR
DO - 10.1080/15421406.2018.1513389
UR - https://doi.org/10.1080/15421406.2018.1513389
TI - The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction
T2 - Molecular Crystals and Liquid Crystals
AU - Glazachev, Eugeny V
AU - Avdontceva, Margarita S.
AU - Asfin, Ruslan E
PY - 2018
DA - 2018/04/13
PB - Taylor & Francis
SP - 219-227
IS - 1
VL - 665
SN - 1542-1406
SN - 1563-5287
SN - 0026-8941
SN - 1056-8816
ER -
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@article{2018_Glazachev,
author = {Eugeny V Glazachev and Margarita S. Avdontceva and Ruslan E Asfin},
title = {The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction},
journal = {Molecular Crystals and Liquid Crystals},
year = {2018},
volume = {665},
publisher = {Taylor & Francis},
month = {apr},
url = {https://doi.org/10.1080/15421406.2018.1513389},
number = {1},
pages = {219--227},
doi = {10.1080/15421406.2018.1513389}
}
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Glazachev, Eugeny V., et al. “The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction.” Molecular Crystals and Liquid Crystals, vol. 665, no. 1, Apr. 2018, pp. 219-227. https://doi.org/10.1080/15421406.2018.1513389.