Taylor & Francis
Synthetic Communications
,  том 40 ,  издание 13 ,  страницы 1985-1991

Efficient Synthesis of 6-(1H-1,2,4-Triazol-1-yl)-thieno[2,3-d]pyrimidin-4(3H)-ones via an Iminophosphorane

Тип публикации: Journal Article
Дата публикации: 2010-06-16
Taylor & Francis
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SJR: 0.322
CiteScore: 4.3
Impact factor: 1.8
ISSN: 00397911, 15322432
Organic Chemistry
Краткое описание
Ethyl 2-amino-4-methyl-5-(1H-1,2,4-triazol-1-yl)thiophene-3-carboxylate 2, obtained from Gewald reaction of 1-(1H-1,2,4-triazol-1-yl)acetone 1 with ethyl cyanoacetate and sulfur, was transferred into iminophosphorane 3. Further reaction of 3 with aromatic isocyanates gave carbodiimides 4, which were treated subsequently with a secondary amine to give 6-(1H-1,2,4-triazol-1-yl)-thieno[2,3-d]pyrimidin-4(3H)-ones 6 in good yields in the presence of a catalytic amount of sodium ethoxide.
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Sun Y. et al. Efficient Synthesis of 6-(1H-1,2,4-Triazol-1-yl)-thieno[2,3-d]pyrimidin-4(3H)-ones via an Iminophosphorane // Synthetic Communications. 2010. Vol. 40. No. 13. pp. 1985-1991.
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Sun Y., Huang N., Ding M. Efficient Synthesis of 6-(1H-1,2,4-Triazol-1-yl)-thieno[2,3-d]pyrimidin-4(3H)-ones via an Iminophosphorane // Synthetic Communications. 2010. Vol. 40. No. 13. pp. 1985-1991.
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TY - JOUR
DO - 10.1080/00397910903219351
UR - https://doi.org/10.1080/00397910903219351
TI - Efficient Synthesis of 6-(1H-1,2,4-Triazol-1-yl)-thieno[2,3-d]pyrimidin-4(3H)-ones via an Iminophosphorane
T2 - Synthetic Communications
AU - Sun, Yong
AU - Huang, Nian-Yu
AU - Ding, Ming-Wu
PY - 2010
DA - 2010/06/16
PB - Taylor & Francis
SP - 1985-1991
IS - 13
VL - 40
SN - 0039-7911
SN - 1532-2432
ER -
BibTex |
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@article{2010_Sun,
author = {Yong Sun and Nian-Yu Huang and Ming-Wu Ding},
title = {Efficient Synthesis of 6-(1H-1,2,4-Triazol-1-yl)-thieno[2,3-d]pyrimidin-4(3H)-ones via an Iminophosphorane},
journal = {Synthetic Communications},
year = {2010},
volume = {40},
publisher = {Taylor & Francis},
month = {jun},
url = {https://doi.org/10.1080/00397910903219351},
number = {13},
pages = {1985--1991},
doi = {10.1080/00397910903219351}
}
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Sun, Yong, et al. “Efficient Synthesis of 6-(1H-1,2,4-Triazol-1-yl)-thieno[2,3-d]pyrimidin-4(3H)-ones via an Iminophosphorane.” Synthetic Communications, vol. 40, no. 13, Jun. 2010, pp. 1985-1991. https://doi.org/10.1080/00397910903219351.