volume 40 issue 23 pages 3452-3466

Total Synthesis of (±)-Armepavines and (±)-Nuciferines From (2-Nitroethenyl)benzene Derivatives

Chia-Fu Chang 1
Chu-Yun Huang 1
Yu Chao Huang 1
Kuan-Yu Lin 1
Yean-Jang Lee 1
Chau-Jong Wang 2
Publication typeJournal Article
Publication date2010-11-03
scimago Q3
wos Q3
SJR0.322
CiteScore4.3
Impact factor1.8
ISSN00397911, 15322432
Organic Chemistry
Abstract
A concise route to armepavine 1 and nuciferine 2 and 3, which can be isolated from the leaves of Nelumbo nucifera (Nymphaceae), has been achieved in which the longest linear sequence is only six steps from commercially available benzaldehyde in 28%, 21%, and 20% overall yield, respectively. The key transformations in the synthesis are the radical cyclization of aryl bromide with Bu3SnH and the Pictet–Spengler reaction of N-substituted amine with aldehyde.
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GOST |
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GOST Copy
Chang C. et al. Total Synthesis of (±)-Armepavines and (±)-Nuciferines From (2-Nitroethenyl)benzene Derivatives // Synthetic Communications. 2010. Vol. 40. No. 23. pp. 3452-3466.
GOST all authors (up to 50) Copy
Chang C., Huang C., Huang Yu. C., Lin K., Lee Y., Wang C. Total Synthesis of (±)-Armepavines and (±)-Nuciferines From (2-Nitroethenyl)benzene Derivatives // Synthetic Communications. 2010. Vol. 40. No. 23. pp. 3452-3466.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1080/00397910903435411
UR - https://doi.org/10.1080/00397910903435411
TI - Total Synthesis of (±)-Armepavines and (±)-Nuciferines From (2-Nitroethenyl)benzene Derivatives
T2 - Synthetic Communications
AU - Chang, Chia-Fu
AU - Huang, Chu-Yun
AU - Huang, Yu Chao
AU - Lin, Kuan-Yu
AU - Lee, Yean-Jang
AU - Wang, Chau-Jong
PY - 2010
DA - 2010/11/03
PB - Taylor & Francis
SP - 3452-3466
IS - 23
VL - 40
SN - 0039-7911
SN - 1532-2432
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2010_Chang,
author = {Chia-Fu Chang and Chu-Yun Huang and Yu Chao Huang and Kuan-Yu Lin and Yean-Jang Lee and Chau-Jong Wang},
title = {Total Synthesis of (±)-Armepavines and (±)-Nuciferines From (2-Nitroethenyl)benzene Derivatives},
journal = {Synthetic Communications},
year = {2010},
volume = {40},
publisher = {Taylor & Francis},
month = {nov},
url = {https://doi.org/10.1080/00397910903435411},
number = {23},
pages = {3452--3466},
doi = {10.1080/00397910903435411}
}
MLA
Cite this
MLA Copy
Chang, Chia-Fu, et al. “Total Synthesis of (±)-Armepavines and (±)-Nuciferines From (2-Nitroethenyl)benzene Derivatives.” Synthetic Communications, vol. 40, no. 23, Nov. 2010, pp. 3452-3466. https://doi.org/10.1080/00397910903435411.