Synthetic Communications

, volume 43 , issue 9 , pages 1314-1327

Palladium-Catalyzed Synthesis of Symmetrical Biaryls Under Microwave Irradiation and Conventional Heating

Abdol R. Hajipour ^{1, 2}

Fatemeh Rafiee ³

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Pharmaceutical Research Laboratory, Department of Chemistry , Isfahan University of Technology , Isfahan , Iran |

Department of Pharmacology , University of Wisconsin, Medical School , Madison , Wisconsin , USA |

Pharmaceutical Research Laboratory, Department of Chemistry, Isfahan University of Technology, Isfahan, Iran |

Publication type: Journal Article

Publication date: 2013-05-03

Taylor & Francis

Synthetic Communications

scimago Q3

wos Q3

SJR: 0.322

CiteScore: 4.3

Impact factor: 1.8

ISSN: 00397911, 15322432

DOI: 10.1080/00397911.2011.632830

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Organic Chemistry

Abstract

The activity of the [Pd{C6H4(CH2N(CH2Ph)2)}(µ-Br)]2 complex was investigated in the synthesis of symmetrical biaryls under both conventional and microwave irradiation conditions, and their results were compared. This complex is efficient, stable, and not sensitive to air or moisture and is a catalyst for the homo-coupling reaction of aryl iodides, bromides, and even chlorides. The products were produced in excellent yields in short reaction times using a catalytic amount of [Pd{C6H4(CH2N(CH2Ph)2)(µ-Br)]2 complex in N-methylpyrolidine (NMP) at 130 °C. In comparison to conventional heating conditions, the reactions under microwave irradiation gave better yields in shorter reaction times.

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Egorova Darya

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DSc in Biological/biomedical sciences, associate professor

62 publications, 439 citations, 2 reviews

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Institute of Ecology and Genetics of Microorganisms of the Ural Branch of the Russian Academy of Sciences

Perm State National Research University

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Hajipour A. R., Rafiee F. Palladium-Catalyzed Synthesis of Symmetrical Biaryls Under Microwave Irradiation and Conventional Heating // Synthetic Communications. 2013. Vol. 43. No. 9. pp. 1314-1327.

GOST all authors (up to 50) Copy

Hajipour A. R., Rafiee F. Palladium-Catalyzed Synthesis of Symmetrical Biaryls Under Microwave Irradiation and Conventional Heating // Synthetic Communications. 2013. Vol. 43. No. 9. pp. 1314-1327.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1080/00397911.2011.632830

UR - https://doi.org/10.1080/00397911.2011.632830

TI - Palladium-Catalyzed Synthesis of Symmetrical Biaryls Under Microwave Irradiation and Conventional Heating

T2 - Synthetic Communications

AU - Hajipour, Abdol R.

AU - Rafiee, Fatemeh

PY - 2013

DA - 2013/05/03

PB - Taylor & Francis

SP - 1314-1327

IS - 9

VL - 43

SN - 0039-7911

SN - 1532-2432

ER -

BibTex |

Cite this

BibTex (up to 50 authors) Copy

@article{2013_Hajipour,

author = {Abdol R. Hajipour and Fatemeh Rafiee},

title = {Palladium-Catalyzed Synthesis of Symmetrical Biaryls Under Microwave Irradiation and Conventional Heating},

journal = {Synthetic Communications},

year = {2013},

volume = {43},

publisher = {Taylor & Francis},

month = {may},

url = {https://doi.org/10.1080/00397911.2011.632830},

number = {9},

pages = {1314--1327},

doi = {10.1080/00397911.2011.632830}

}

MLA

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MLA Copy

Hajipour, Abdol R., et al. “Palladium-Catalyzed Synthesis of Symmetrical Biaryls Under Microwave Irradiation and Conventional Heating.” Synthetic Communications, vol. 43, no. 9, May. 2013, pp. 1314-1327. https://doi.org/10.1080/00397911.2011.632830.

Publisher

Taylor & Francis

Journal

Synthetic Communications

scimago Q3

wos Q3

SJR

0.322

CiteScore

4.3

Impact factor

1.8

ISSN

00397911 (Print)

15322432 (Electronic)