Catalysis by Amberlyst A-21: A Greener Approach to 4,5,6,7-Tetrahydro-1H-indazol-3(2H)-ones via Construction of Cyclohexanones
Manam Sreenivasa Rao
1
,
Meda Haritha
2
,
Sunder Kumar Kolli
3
,
Mandava V. Basaveswara Rao
4
,
Manojit Pal
5
1
a C.R.College, Ganapavaram , Chilakaluripet , Andhra Pradesh , India
|
2
b Department of Pharmacy , Krishna University , Machilipatnam , Andhra Pradesh , India
|
4
d Department of Chemistry , Krishna University , Nuzvid , Andhra Pradesh , India
|
Тип публикации: Journal Article
Дата публикации: 2014-03-19
scimago Q3
wos Q3
БС2
SJR: 0.322
CiteScore: 4.3
Impact factor: 1.8
ISSN: 00397911, 15322432
Organic Chemistry
Краткое описание
The 4,5,6,7-tetrahydro-1H-indazol-3(2H)-one derivatives have been synthesized in good yields via a two-step method in a single pot. The initial step involved the construction of cyclohexanone ring from aromatic aldehydes and β-ketoester in i-PrOH using an inexpensive and reusable catalyst (i.e., Amberlyst A-21) under mild reaction conditions. The utility of this catalyst has been demonstrated in synthesizing a range of cyclohexanone derivatives. The catalyst can be recovered and recycled, which makes this procedure simple, convenient, economically viable, and environmental friendly. [Supplementary materials are available for this article. Go to the publisher's online edition of Synthetic Communications® for the following free supplemental resource(s): Full experimental and spectral details.]
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Rao M. S. et al. Catalysis by Amberlyst A-21: A Greener Approach to 4,5,6,7-Tetrahydro-1H-indazol-3(2H)-ones via Construction of Cyclohexanones // Synthetic Communications. 2014. Vol. 44. No. 8. pp. 1076-1083.
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Rao M. S., Haritha M., Kolli S. K., Basaveswara Rao M. V., Pal M. Catalysis by Amberlyst A-21: A Greener Approach to 4,5,6,7-Tetrahydro-1H-indazol-3(2H)-ones via Construction of Cyclohexanones // Synthetic Communications. 2014. Vol. 44. No. 8. pp. 1076-1083.
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TY - JOUR
DO - 10.1080/00397911.2013.844260
UR - https://doi.org/10.1080/00397911.2013.844260
TI - Catalysis by Amberlyst A-21: A Greener Approach to 4,5,6,7-Tetrahydro-1H-indazol-3(2H)-ones via Construction of Cyclohexanones
T2 - Synthetic Communications
AU - Rao, Manam Sreenivasa
AU - Haritha, Meda
AU - Kolli, Sunder Kumar
AU - Basaveswara Rao, Mandava V.
AU - Pal, Manojit
PY - 2014
DA - 2014/03/19
PB - Taylor & Francis
SP - 1076-1083
IS - 8
VL - 44
SN - 0039-7911
SN - 1532-2432
ER -
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@article{2014_Rao,
author = {Manam Sreenivasa Rao and Meda Haritha and Sunder Kumar Kolli and Mandava V. Basaveswara Rao and Manojit Pal},
title = {Catalysis by Amberlyst A-21: A Greener Approach to 4,5,6,7-Tetrahydro-1H-indazol-3(2H)-ones via Construction of Cyclohexanones},
journal = {Synthetic Communications},
year = {2014},
volume = {44},
publisher = {Taylor & Francis},
month = {mar},
url = {https://doi.org/10.1080/00397911.2013.844260},
number = {8},
pages = {1076--1083},
doi = {10.1080/00397911.2013.844260}
}
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Rao, Manam Sreenivasa, et al. “Catalysis by Amberlyst A-21: A Greener Approach to 4,5,6,7-Tetrahydro-1H-indazol-3(2H)-ones via Construction of Cyclohexanones.” Synthetic Communications, vol. 44, no. 8, Mar. 2014, pp. 1076-1083. https://doi.org/10.1080/00397911.2013.844260.