Synthetic Communications

, том 26 , издание 14 , страницы 2775-2781

An Improved Method for the Preparation OF 3,5-Difluorosalicylaldehyde and 3,5-Difluorosalicylic Acid^#

Тип публикации: Journal Article

Дата публикации: 1996-07-01

Taylor & Francis

Synthetic Communications

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SJR: 0.322

CiteScore: 4.3

Impact factor: 1.8

ISSN: 00397911, 15322432

DOI: 10.1080/00397919608004595

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Organic Chemistry

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An improved method for the synthesis of 3,5-difluorosalicylic acid (3b) and 3,5-difluorosalicylaldehyde (3a) is described. 2,4-Difluorophenol (4) undergoes a formylation reaction to afford aldehyde 3a which is oxidized to the desired acid 3b. This method avoids the use of the highly corrosive HF and fluorine gas and requires no special laboratory apparatus. #Dedicated to the memory of Rosemarie R. Ungarelli, Academic Advisor, Chemistry Department, Long Island Univeristy, C.W. Post Center.

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Журналы

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Bioorganic and Medicinal Chemistry Letters	Bioorganic and Medicinal Chemistry Letters, 2, 22.22% Bioorganic and Medicinal Chemistry Letters 2 публикации, 22.22%
Synthesis	Synthesis, 2, 22.22% Synthesis 2 публикации, 22.22%
Bulletin of the Chemical Society of Japan	Bulletin of the Chemical Society of Japan, 1, 11.11% Bulletin of the Chemical Society of Japan 1 публикация, 11.11%
Canadian Journal of Chemistry	Canadian Journal of Chemistry, 1, 11.11% Canadian Journal of Chemistry 1 публикация, 11.11%
Journal of Fluorine Chemistry	Journal of Fluorine Chemistry, 1, 11.11% Journal of Fluorine Chemistry 1 публикация, 11.11%
Synthetic Communications	Synthetic Communications, 1, 11.11% Synthetic Communications 1 публикация, 11.11%
Russian Chemical Reviews	Russian Chemical Reviews, 1, 11.11% Russian Chemical Reviews 1 публикация, 11.11%
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Elsevier	Elsevier, 3, 33.33% Elsevier 3 публикации, 33.33%
Georg Thieme Verlag KG	Georg Thieme Verlag KG, 2, 22.22% Georg Thieme Verlag KG 2 публикации, 22.22%
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Taylor & Francis	Taylor & Francis, 1, 11.11% Taylor & Francis 1 публикация, 11.11%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 11.11% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 публикация, 11.11%
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Weidner-Wells M. A., Fraga-Spano S. A. An Improved Method for the Preparation OF 3,5-Difluorosalicylaldehyde and 3,5-Difluorosalicylic Acid# // Synthetic Communications. 1996. Vol. 26. No. 14. pp. 2775-2781.

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TY - JOUR

DO - 10.1080/00397919608004595

UR - https://doi.org/10.1080/00397919608004595

TI - An Improved Method for the Preparation OF 3,5-Difluorosalicylaldehyde and 3,5-Difluorosalicylic Acid#

T2 - Synthetic Communications

AU - Weidner-Wells, Michele A

AU - Fraga-Spano, Stephanie A

PY - 1996

DA - 1996/07/01

PB - Taylor & Francis

SP - 2775-2781

IS - 14

VL - 26

SN - 0039-7911

SN - 1532-2432

ER -

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@article{1996_Weidner-Wells,

author = {Michele A Weidner-Wells and Stephanie A Fraga-Spano},

title = {An Improved Method for the Preparation OF 3,5-Difluorosalicylaldehyde and 3,5-Difluorosalicylic Acid#},

journal = {Synthetic Communications},

year = {1996},

volume = {26},

publisher = {Taylor & Francis},

month = {jul},

url = {https://doi.org/10.1080/00397919608004595},

number = {14},

pages = {2775--2781},

doi = {10.1080/00397919608004595}

}

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Weidner-Wells, Michele A., and Stephanie A Fraga-Spano. “An Improved Method for the Preparation OF 3,5-Difluorosalicylaldehyde and 3,5-Difluorosalicylic Acid#.” Synthetic Communications, vol. 26, no. 14, Jul. 1996, pp. 2775-2781. https://doi.org/10.1080/00397919608004595.