Triple insertion of ethylisocyanate into a W-Cl bond and its inner-sphere cyclization. Crystal structure of tetrachlorooxo (3,5-diethyl-2-methylamino[1,3,5]-oxadiazine-2,4-dione) tungsten(VI)
Тип публикации: Journal Article
Дата публикации: 2003-07-01
scimago Q3
wos Q3
БС2
SJR: 0.294
CiteScore: 3.4
Impact factor: 2.1
ISSN: 00958972, 10290389
Materials Chemistry
Physical and Theoretical Chemistry
Краткое описание
The insertion product [WCl5{N(Et)C(O)OC(NEt)N(Et)C(O)Cl}] (I) is obtained by the room-temperature reaction of WCl6 with an excess of EtNCO in dichloroethane. The structure of the chain ligand in I is deduced from an IR study and the results of X-ray diffraction analyses of crystals of an oxo-complex, WOCI4{OCN(Et)C(O)N(Et)C(NHEt)O} (II), which is obtained by partial hydrolysis of I.
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Ovchinnikova N. et al. Triple insertion of ethylisocyanate into a W-Cl bond and its inner-sphere cyclization. Crystal structure of tetrachlorooxo (3,5-diethyl-2-methylamino[1,3,5]-oxadiazine-2,4-dione) tungsten(VI) // Journal of Coordination Chemistry. 2003. Vol. 56. No. 11. pp. 995-1002.
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Ovchinnikova N., Sinyakov A. E., Sergienko V. S., Alexandrov G., Burtzev M. Yu. Triple insertion of ethylisocyanate into a W-Cl bond and its inner-sphere cyclization. Crystal structure of tetrachlorooxo (3,5-diethyl-2-methylamino[1,3,5]-oxadiazine-2,4-dione) tungsten(VI) // Journal of Coordination Chemistry. 2003. Vol. 56. No. 11. pp. 995-1002.
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TY - JOUR
DO - 10.1080/00958970310001593406
UR - https://doi.org/10.1080/00958970310001593406
TI - Triple insertion of ethylisocyanate into a W-Cl bond and its inner-sphere cyclization. Crystal structure of tetrachlorooxo (3,5-diethyl-2-methylamino[1,3,5]-oxadiazine-2,4-dione) tungsten(VI)
T2 - Journal of Coordination Chemistry
AU - Ovchinnikova, N.A.
AU - Sinyakov, A E
AU - Sergienko, V S
AU - Alexandrov, G.G.
AU - Burtzev, M Yu
PY - 2003
DA - 2003/07/01
PB - Taylor & Francis
SP - 995-1002
IS - 11
VL - 56
SN - 0095-8972
SN - 1029-0389
ER -
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@article{2003_Ovchinnikova,
author = {N.A. Ovchinnikova and A E Sinyakov and V S Sergienko and G.G. Alexandrov and M Yu Burtzev},
title = {Triple insertion of ethylisocyanate into a W-Cl bond and its inner-sphere cyclization. Crystal structure of tetrachlorooxo (3,5-diethyl-2-methylamino[1,3,5]-oxadiazine-2,4-dione) tungsten(VI)},
journal = {Journal of Coordination Chemistry},
year = {2003},
volume = {56},
publisher = {Taylor & Francis},
month = {jul},
url = {https://doi.org/10.1080/00958970310001593406},
number = {11},
pages = {995--1002},
doi = {10.1080/00958970310001593406}
}
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Ovchinnikova, N.A., et al. “Triple insertion of ethylisocyanate into a W-Cl bond and its inner-sphere cyclization. Crystal structure of tetrachlorooxo (3,5-diethyl-2-methylamino[1,3,5]-oxadiazine-2,4-dione) tungsten(VI).” Journal of Coordination Chemistry, vol. 56, no. 11, Jul. 2003, pp. 995-1002. https://doi.org/10.1080/00958970310001593406.
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