volume 58 issue 4 pages 295-300

Ligation to tin(IV) organometallics: crystal structure of tribenzyl(chloro)(4-N,N′-dimethylaminopyridine)tin(IV)

Publication typeJournal Article
Publication date2005-03-10
scimago Q3
wos Q3
SJR0.294
CiteScore3.4
Impact factor2.1
ISSN00958972, 10290389
Materials Chemistry
Physical and Theoretical Chemistry
Abstract
The preparation and characterization of the air-stable, five-coordinate complex of 4-(dimethylamino)pyridine with tribenzyltin chloride is reported. The complex crystallizes in space group P21/n with a = 10.3743(17), b = 24.356(17), c = 10.628(2) A, β = 102.504(15)°. Single crystal X-ray analysis confirms the structure to be monomeric in which the geometry around tin is a trigonal bipyramid with equatorial benzyl groups. The 119Sn NMR signal of the complex in CDCl3 occurs upfield with respect to the corresponding signal in (C6H5CH2)3SnCl, indicating lack of dissociation of the ligand in solution. Computations using the PM3 hamiltonian for the complex yielded a trigonal bipyramidal structure with satisfactory agreement in metrical parameters with those obtained from X-ray analysis.
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Chandrasekar S. et al. Ligation to tin(IV) organometallics: crystal structure of tribenzyl(chloro)(4-N,N′-dimethylaminopyridine)tin(IV) // Journal of Coordination Chemistry. 2005. Vol. 58. No. 4. pp. 295-300.
GOST all authors (up to 50) Copy
Chandrasekar S., Krishnamoorthy B. S., Sridevi V. S., Panchanatheswaran K. Ligation to tin(IV) organometallics: crystal structure of tribenzyl(chloro)(4-N,N′-dimethylaminopyridine)tin(IV) // Journal of Coordination Chemistry. 2005. Vol. 58. No. 4. pp. 295-300.
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RIS Copy
TY - JOUR
DO - 10.1080/00958970512331325520
UR - https://doi.org/10.1080/00958970512331325520
TI - Ligation to tin(IV) organometallics: crystal structure of tribenzyl(chloro)(4-N,N′-dimethylaminopyridine)tin(IV)
T2 - Journal of Coordination Chemistry
AU - Chandrasekar, S.
AU - Krishnamoorthy, B S
AU - Sridevi, V S
AU - Panchanatheswaran, K.
PY - 2005
DA - 2005/03/10
PB - Taylor & Francis
SP - 295-300
IS - 4
VL - 58
SN - 0095-8972
SN - 1029-0389
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2005_Chandrasekar,
author = {S. Chandrasekar and B S Krishnamoorthy and V S Sridevi and K. Panchanatheswaran},
title = {Ligation to tin(IV) organometallics: crystal structure of tribenzyl(chloro)(4-N,N′-dimethylaminopyridine)tin(IV)},
journal = {Journal of Coordination Chemistry},
year = {2005},
volume = {58},
publisher = {Taylor & Francis},
month = {mar},
url = {https://doi.org/10.1080/00958970512331325520},
number = {4},
pages = {295--300},
doi = {10.1080/00958970512331325520}
}
MLA
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Chandrasekar, S., et al. “Ligation to tin(IV) organometallics: crystal structure of tribenzyl(chloro)(4-N,N′-dimethylaminopyridine)tin(IV).” Journal of Coordination Chemistry, vol. 58, no. 4, Mar. 2005, pp. 295-300. https://doi.org/10.1080/00958970512331325520.