Synthesis, structure, and magnetic properties of lanthanide ferrocenoylacetonates with nitrate and 2,2′-bipyridine ligands
Pavel S Koroteev
1
,
P S Koroteev
1
,
Zh V Dobrokhotova
1
,
A. B. Ilyukhin
1
,
N. N. Efimov
1
,
V. M. Novotortsev
1
Publication type: Journal Article
Publication date: 2016-08-05
scimago Q3
wos Q3
SJR: 0.294
CiteScore: 3.4
Impact factor: 2.1
ISSN: 00958972, 10290389
Materials Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract Ferrocenoylacetonate complexes of several lanthanides, [Ln(fca)2(NO3)(bpy)]·nMeC6H5 (Ln = Sm (1), Dy (3), Er (4), Yb (5), n = 1; Eu (2), n = 0.5; fca = FcC(O)CHC(O)Me; bpy = 2,2′-bipyridine), were synthesized and characterized by X-ray single-crystal analysis. Complexes 1, 4, and 5 are isostructural; 2 has a similar molecular structure with cis-disposition of fca ligands. The molecular structure of 3 is different, with trans-disposition of the fca ligands. Crystal lattices of the complexes are stabilized by π-stacking interactions. The Ln3+ ions in the complexes are eight-coordinate. According to mass spectroscopic data, the complexes are unstable in the gas phase. Magnetic properties of 2 and 4 were studied in a DC field; for 4, AC studies were also carried out. The values of spin-orbital parameters obtained using two estimation methods for 2 are in satisfactory agreement. Slow relaxation of the magnetization was found for the Er complex.
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Koroteev P. S. et al. Synthesis, structure, and magnetic properties of lanthanide ferrocenoylacetonates with nitrate and 2,2′-bipyridine ligands // Journal of Coordination Chemistry. 2016. Vol. 69. No. 18. pp. 2723-2735.
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Koroteev P. S., Koroteev P. S., Dobrokhotova Z. V., Ilyukhin A. B., Efimov N. N., Efimov N. N., Novotortsev V. M. Synthesis, structure, and magnetic properties of lanthanide ferrocenoylacetonates with nitrate and 2,2′-bipyridine ligands // Journal of Coordination Chemistry. 2016. Vol. 69. No. 18. pp. 2723-2735.
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TY - JOUR
DO - 10.1080/00958972.2016.1217409
UR - https://www.tandfonline.com/doi/full/10.1080/00958972.2016.1217409
TI - Synthesis, structure, and magnetic properties of lanthanide ferrocenoylacetonates with nitrate and 2,2′-bipyridine ligands
T2 - Journal of Coordination Chemistry
AU - Koroteev, Pavel S
AU - Koroteev, P S
AU - Dobrokhotova, Zh V
AU - Ilyukhin, A. B.
AU - Efimov, Nikolay N.
AU - Efimov, N. N.
AU - Novotortsev, V. M.
PY - 2016
DA - 2016/08/05
PB - Taylor & Francis
SP - 2723-2735
IS - 18
VL - 69
SN - 0095-8972
SN - 1029-0389
ER -
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BibTex (up to 50 authors)
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@article{2016_Koroteev,
author = {Pavel S Koroteev and P S Koroteev and Zh V Dobrokhotova and A. B. Ilyukhin and Nikolay N. Efimov and N. N. Efimov and V. M. Novotortsev},
title = {Synthesis, structure, and magnetic properties of lanthanide ferrocenoylacetonates with nitrate and 2,2′-bipyridine ligands},
journal = {Journal of Coordination Chemistry},
year = {2016},
volume = {69},
publisher = {Taylor & Francis},
month = {aug},
url = {https://www.tandfonline.com/doi/full/10.1080/00958972.2016.1217409},
number = {18},
pages = {2723--2735},
doi = {10.1080/00958972.2016.1217409}
}
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MLA
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Koroteev, Pavel S., et al. “Synthesis, structure, and magnetic properties of lanthanide ferrocenoylacetonates with nitrate and 2,2′-bipyridine ligands.” Journal of Coordination Chemistry, vol. 69, no. 18, Aug. 2016, pp. 2723-2735. https://www.tandfonline.com/doi/full/10.1080/00958972.2016.1217409.