On-line coupling of solid-phase extraction of phenols on porous graphitic carbon and LC separation on C18 silica gel column via subcritical water desorption
Publication type: Journal Article
Publication date: 2016-06-17
scimago Q2
wos Q3
SJR: 0.443
CiteScore: 5.4
Impact factor: 2.3
ISSN: 01496395, 15205754
General Chemistry
General Chemical Engineering
Process Chemistry and Technology
Filtration and Separation
Abstract
ABSTRACTAn approach to the on-line coupling of solid-phase extraction on porous graphitic carbon (PGC) column and high performance liquid chromatography (HPLC) separation on octadecyl silica column is proposed. The approach includes extraction of phenols from 10 ml of water sample on PGC column; desorption with subcritical water at 175°C, injection of the eluate to the HPLC column and separation at ambient temperature with acetonitrile–water eluent. Limits of detection for UV detection of phenols were 1–5 μg l−1, and analyte peaks were 20–50% narrower than for direct injection of 20 μl of sample.
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GOST
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Borisova D. R. et al. On-line coupling of solid-phase extraction of phenols on porous graphitic carbon and LC separation on C18 silica gel column via subcritical water desorption // Separation Science and Technology. 2016. Vol. 51. No. 12. pp. 1979-1985.
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Borisova D. R., Statkus M. A., Tsysin G. I., Zolotov Y. A. On-line coupling of solid-phase extraction of phenols on porous graphitic carbon and LC separation on C18 silica gel column via subcritical water desorption // Separation Science and Technology. 2016. Vol. 51. No. 12. pp. 1979-1985.
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RIS
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TY - JOUR
DO - 10.1080/01496395.2016.1199571
UR - https://www.tandfonline.com/doi/full/10.1080/01496395.2016.1199571
TI - On-line coupling of solid-phase extraction of phenols on porous graphitic carbon and LC separation on C18 silica gel column via subcritical water desorption
T2 - Separation Science and Technology
AU - Borisova, Dina Rashidovna
AU - Statkus, Mikhail Alexandrovich
AU - Tsysin, Grigory Ilyich
AU - Zolotov, Yury Alexandrovich
PY - 2016
DA - 2016/06/17
PB - Taylor & Francis
SP - 1979-1985
IS - 12
VL - 51
SN - 0149-6395
SN - 1520-5754
ER -
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BibTex (up to 50 authors)
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@article{2016_Borisova,
author = {Dina Rashidovna Borisova and Mikhail Alexandrovich Statkus and Grigory Ilyich Tsysin and Yury Alexandrovich Zolotov},
title = {On-line coupling of solid-phase extraction of phenols on porous graphitic carbon and LC separation on C18 silica gel column via subcritical water desorption},
journal = {Separation Science and Technology},
year = {2016},
volume = {51},
publisher = {Taylor & Francis},
month = {jun},
url = {https://www.tandfonline.com/doi/full/10.1080/01496395.2016.1199571},
number = {12},
pages = {1979--1985},
doi = {10.1080/01496395.2016.1199571}
}
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MLA
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Borisova, Dina Rashidovna, et al. “On-line coupling of solid-phase extraction of phenols on porous graphitic carbon and LC separation on C18 silica gel column via subcritical water desorption.” Separation Science and Technology, vol. 51, no. 12, Jun. 2016, pp. 1979-1985. https://www.tandfonline.com/doi/full/10.1080/01496395.2016.1199571.
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