Synthesis and Characterization of Itaconyl Chloride
Publication type: Journal Article
Publication date: 2019-04-10
SJR: —
CiteScore: —
Impact factor: —
ISSN: 17578981, 1757899X
General Medicine
Abstract
Itaconyl chloride was synthesised using the bio-based itaconic acid (IA) and phosphorus pentachloride (PCl5) as raw material by a molten method. The effects of various main factors, i.e. The solvent effect on the quality of the product during the purifying process was studied. The ratio of raw materials, the vacuum distillation temperature and vacuum distillation time on itaconyl chloride preparation were investigated. The optimum conditions of synthesis were determined as f ollows: toluene as purified solvent, n(PCl5):n(IA) = 2.15:1, the vacuum distillation temperature 80 °C, the vacuum distillation time 2 h. The yield of itaconyl chloride could reach 90 % and its purity was more than 98 %. The structure of itaconyl chloride was confirmed by means of Fourier Transform Infra-Red (FT-IR) and Nuclear magnetic resonance hydrogen spectrum (1H-NMR).
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Zeng X. et al. Synthesis and Characterization of Itaconyl Chloride // IOP Conference Series: Materials Science and Engineering. 2019. Vol. 490. p. 22052.
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Zeng X., Xu G., Wang P., Wang C. Synthesis and Characterization of Itaconyl Chloride // IOP Conference Series: Materials Science and Engineering. 2019. Vol. 490. p. 22052.
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TY - JOUR
DO - 10.1088/1757-899x/490/2/022052
UR - https://doi.org/10.1088/1757-899x/490/2/022052
TI - Synthesis and Characterization of Itaconyl Chloride
T2 - IOP Conference Series: Materials Science and Engineering
AU - Zeng, Xueqi
AU - Xu, GuoJing
AU - Wang, Pengfei
AU - Wang, Chuanxing
PY - 2019
DA - 2019/04/10
PB - IOP Publishing
SP - 22052
VL - 490
SN - 1757-8981
SN - 1757-899X
ER -
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@article{2019_Zeng,
author = {Xueqi Zeng and GuoJing Xu and Pengfei Wang and Chuanxing Wang},
title = {Synthesis and Characterization of Itaconyl Chloride},
journal = {IOP Conference Series: Materials Science and Engineering},
year = {2019},
volume = {490},
publisher = {IOP Publishing},
month = {apr},
url = {https://doi.org/10.1088/1757-899x/490/2/022052},
pages = {22052},
doi = {10.1088/1757-899x/490/2/022052}
}