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том 64 издание 2 страницы o501-o502

4′-Amino-2,2′′-dioxo-2,2′′,3,3′′-tetrahydro-1H-indole-3-spiro-1′-cyclopent-3′-ene-2′-spiro-3′′-1H-indole-3′,5′,5′-tricarbonitrile dihydrate

Тип публикацииJournal Article
Дата публикации2008-01-23
General Chemistry
Condensed Matter Physics
General Materials Science
Краткое описание
In the title compound, C(22)H(12)N(6)O(2)·2H(2)O, the cyclo-pentene ring adopts an envelope conformation, with the spiro C atom bonded to the dicyano-substituted C atom deviating by 0.437 (2) Å from the plane of the remaining four atoms in the ring. The puckering and smallest displacement asymmetry parameters for the ring are q(2) = 0.275 (2) Å, ϕ = 212.4 (4)° and Δ(s)(C(2)) = 2.7 (2). The dihedral angle between the two indole groups is 60.1 (1)°. The structure contains inter-molecular N-H⋯O hydrogen bonds involving the indole groups and O-H⋯O and O-H⋯N hydrogen bonds involving the water mol-ecules.
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Acta Crystallographica Section E Structure Reports Online
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Tetrahedron Letters
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Acta Crystallographica Section E: Crystallographic Communications
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International Union of Crystallography (IUCr)
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Elsevier
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Gayathri D. et al. 4′-Amino-2,2′′-dioxo-2,2′′,3,3′′-tetrahydro-1H-indole-3-spiro-1′-cyclopent-3′-ene-2′-spiro-3′′-1H-indole-3′,5′,5′-tricarbonitrile dihydrate // Acta Crystallographica Section E Structure Reports Online. 2008. Vol. 64. No. 2. p. o501-o502.
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Gayathri D., Velmurugan D., Shanthi G., Perumal P. T., Ravikumar K. 4′-Amino-2,2′′-dioxo-2,2′′,3,3′′-tetrahydro-1H-indole-3-spiro-1′-cyclopent-3′-ene-2′-spiro-3′′-1H-indole-3′,5′,5′-tricarbonitrile dihydrate // Acta Crystallographica Section E Structure Reports Online. 2008. Vol. 64. No. 2. p. o501-o502.
RIS |
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TY - JOUR
DO - 10.1107/s1600536808002146
UR - https://doi.org/10.1107/s1600536808002146
TI - 4′-Amino-2,2′′-dioxo-2,2′′,3,3′′-tetrahydro-1H-indole-3-spiro-1′-cyclopent-3′-ene-2′-spiro-3′′-1H-indole-3′,5′,5′-tricarbonitrile dihydrate
T2 - Acta Crystallographica Section E Structure Reports Online
AU - Gayathri, D.
AU - Velmurugan, D.
AU - Shanthi, G.
AU - Perumal, Paramasivam Thirumalai
AU - Ravikumar, K.
PY - 2008
DA - 2008/01/23
PB - International Union of Crystallography (IUCr)
SP - o501-o502
IS - 2
VL - 64
PMID - 21201522
SN - 1600-5368
ER -
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@article{2008_Gayathri,
author = {D. Gayathri and D. Velmurugan and G. Shanthi and Paramasivam Thirumalai Perumal and K. Ravikumar},
title = {4′-Amino-2,2′′-dioxo-2,2′′,3,3′′-tetrahydro-1H-indole-3-spiro-1′-cyclopent-3′-ene-2′-spiro-3′′-1H-indole-3′,5′,5′-tricarbonitrile dihydrate},
journal = {Acta Crystallographica Section E Structure Reports Online},
year = {2008},
volume = {64},
publisher = {International Union of Crystallography (IUCr)},
month = {jan},
url = {https://doi.org/10.1107/s1600536808002146},
number = {2},
pages = {o501--o502},
doi = {10.1107/s1600536808002146}
}
MLA
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Gayathri, D., et al. “4′-Amino-2,2′′-dioxo-2,2′′,3,3′′-tetrahydro-1H-indole-3-spiro-1′-cyclopent-3′-ene-2′-spiro-3′′-1H-indole-3′,5′,5′-tricarbonitrile dihydrate.” Acta Crystallographica Section E Structure Reports Online, vol. 64, no. 2, Jan. 2008, pp. o501-o502. https://doi.org/10.1107/s1600536808002146.
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