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N′-(3,5-Dibromo-2-hydroxybenzylidene)-4-nitrobenzohydrazide methanol monosolvate
Publication type: Journal Article
Publication date: 2011-08-11
SJR: —
CiteScore: —
Impact factor: —
ISSN: 16005368
PubMed ID:
22065140
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
The title compound, C14H9Br2N3O4·CH4O, was obtained as the product of the reaction of 3,5-dibromosalicylaldehyde with 4-nitrobenzohydrazide in methanol. The benzohydrazide molecule is nearly planar, with a maximum deviation of 0.126 (2) Å. The mean planes of the two benzene rings make a dihedral angle of 9.3 (3)°. Intramolecular O—H⋯N and O—H⋯Br interactions are observed in the benzohydrazide molecule. In the crystal, pairs of adjacent benzohydrazide molecules are linked by two methanol molecules through intermolecular O—H⋯O and N—H⋯O hydrogen bonds, forming a dimer.
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Acta Crystallographica Section E Structure Reports Online
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International Union of Crystallography (IUCr)
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Zhou X. et al. N′-(3,5-Dibromo-2-hydroxybenzylidene)-4-nitrobenzohydrazide methanol monosolvate // Acta Crystallographica Section E Structure Reports Online. 2011. Vol. 67. No. 9. p. o2275.
GOST all authors (up to 50)
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Zhou X., Zhou X., Gao S., Ma J. N′-(3,5-Dibromo-2-hydroxybenzylidene)-4-nitrobenzohydrazide methanol monosolvate // Acta Crystallographica Section E Structure Reports Online. 2011. Vol. 67. No. 9. p. o2275.
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RIS
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TY - JOUR
DO - 10.1107/s1600536811031187
UR - https://doi.org/10.1107/s1600536811031187
TI - N′-(3,5-Dibromo-2-hydroxybenzylidene)-4-nitrobenzohydrazide methanol monosolvate
T2 - Acta Crystallographica Section E Structure Reports Online
AU - Zhou, Xin
AU - Zhou, Xin
AU - Gao, Shu-tao
AU - Ma, Jing-Jun
PY - 2011
DA - 2011/08/11
PB - International Union of Crystallography (IUCr)
SP - o2275
IS - 9
VL - 67
PMID - 22065140
SN - 1600-5368
ER -
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BibTex (up to 50 authors)
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@article{2011_Zhou,
author = {Xin Zhou and Xin Zhou and Shu-tao Gao and Jing-Jun Ma},
title = {N′-(3,5-Dibromo-2-hydroxybenzylidene)-4-nitrobenzohydrazide methanol monosolvate},
journal = {Acta Crystallographica Section E Structure Reports Online},
year = {2011},
volume = {67},
publisher = {International Union of Crystallography (IUCr)},
month = {aug},
url = {https://doi.org/10.1107/s1600536811031187},
number = {9},
pages = {o2275},
doi = {10.1107/s1600536811031187}
}
Cite this
MLA
Copy
Zhou, Xin, et al. “N′-(3,5-Dibromo-2-hydroxybenzylidene)-4-nitrobenzohydrazide methanol monosolvate.” Acta Crystallographica Section E Structure Reports Online, vol. 67, no. 9, Aug. 2011, p. o2275. https://doi.org/10.1107/s1600536811031187.