,
volume 60
,
issue 9
,
pages m440-m442
μ-Biphenyl-2,2′-dithiolato-′K 2S:S′-bis[(triphenylphosphine-KP)gold(I)]
Publication type: Journal Article
Publication date: 2004-08-11
SJR: —
CiteScore: —
Impact factor: —
ISSN: 01082701, 16005759
PubMed ID:
15345827
General Biochemistry, Genetics and Molecular Biology
General Medicine
Abstract
The reaction of ClAuPPh3 and 1,1′-biphenyl-2,2′-dithiol in the presence of trimethylbenzylammonium chloride and K2CO3 in a tetrahydrofuran/methanol solution gives the title complex, [Au2(C12H8S2)(C18H15P)2]. The molecule contains P—Au—S units which `cross' with torsion angles of ∼90° [P—Au—Au—P = 86.23 (5)° and S—Au—Au—S = 95.62 (5)°]. The intra- and intermolecular Au⋯Au distances [3.9064 (3) and 6.3797 (5) A, respectively] are outside the range for typical Au⋯Au interactions. However, the Au atoms appear to be drawn together, leading to a significant bending of the P—Au—S angles [170.24 (5) and 169.52 (5)°].
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Larkin S. A. et al. μ-Biphenyl-2,2′-dithiolato-′K 2S:S′-bis[(triphenylphosphine-KP)gold(I)] // Acta Crystallographica Section C Crystal Structure Communications. 2004. Vol. 60. No. 9. p. m440-m442.
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Larkin S. A., Krause Bauer J. A., Konoplev V. E., Dyadchenko V. P., Lemenovskii D. A., Bruce M. R. M., Bruce A. E. μ-Biphenyl-2,2′-dithiolato-′K 2S:S′-bis[(triphenylphosphine-KP)gold(I)] // Acta Crystallographica Section C Crystal Structure Communications. 2004. Vol. 60. No. 9. p. m440-m442.
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TY - JOUR
DO - 10.1107/S0108270104016099
UR - https://scripts.iucr.org/cgi-bin/paper?S0108270104016099
TI - μ-Biphenyl-2,2′-dithiolato-′K 2S:S′-bis[(triphenylphosphine-KP)gold(I)]
T2 - Acta Crystallographica Section C Crystal Structure Communications
AU - Larkin, Scott A.
AU - Krause Bauer, Jeanette A.
AU - Konoplev, V. E.
AU - Dyadchenko, Victor P.
AU - Lemenovskii, Dmitrii A.
AU - Bruce, Mitchell R. M.
AU - Bruce, Alice E.
PY - 2004
DA - 2004/08/11
PB - International Union of Crystallography (IUCr)
SP - m440-m442
IS - 9
VL - 60
PMID - 15345827
SN - 0108-2701
SN - 1600-5759
ER -
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@article{2004_Larkin,
author = {Scott A. Larkin and Jeanette A. Krause Bauer and V. E. Konoplev and Victor P. Dyadchenko and Dmitrii A. Lemenovskii and Mitchell R. M. Bruce and Alice E. Bruce},
title = {μ-Biphenyl-2,2′-dithiolato-′K 2S:S′-bis[(triphenylphosphine-KP)gold(I)]},
journal = {Acta Crystallographica Section C Crystal Structure Communications},
year = {2004},
volume = {60},
publisher = {International Union of Crystallography (IUCr)},
month = {aug},
url = {https://scripts.iucr.org/cgi-bin/paper?S0108270104016099},
number = {9},
pages = {m440--m442},
doi = {10.1107/S0108270104016099}
}
Cite this
MLA
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Larkin, Scott A., et al. “μ-Biphenyl-2,2′-dithiolato-′K 2S:S′-bis[(triphenylphosphine-KP)gold(I)].” Acta Crystallographica Section C Crystal Structure Communications, vol. 60, no. 9, Aug. 2004, pp. m440-m442. https://scripts.iucr.org/cgi-bin/paper?S0108270104016099.