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International Union of Crystallography (IUCr)
Acta Crystallographica Section E Structure Reports Online
,  том 69 ,  издание 11 ,  страницы m626-m627

Di-μ-oxido-bis(2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)] diphenolatotitanium(IV)) chloroform disolvate

Тип публикации: Journal Article
Дата публикации: 2013-10-31
International Union of Crystallography (IUCr)
SJR: —
CiteScore: —
Impact factor: —
ISSN: 16005368
General Chemistry
Condensed Matter Physics
General Materials Science
Краткое описание

In the title compound, [Ti2(C16H14N2O2)2O2]·2CHCl3, the TiIVatom in the centrosymmetric complex has a distorted octahedral N2O4coordination environment and is linkedviatwo μ2-oxido bridges into a dinuclear centrosymmetric complex, with a Ti...Ti separation of 2.7794 (8) Å. In the salen (N,N′-ethylenebis(salicylimine)) ligand, the two salicylimine units make a dihedral angle of 45.31 (5)°. The complex molecules are stacked parallel to [100], forming channels in which the solvent chloroform molecules are located. C—H...O hydrogen-bonding interactions between the complex molecules and the solvent molecules consolidate the crystal packing.

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Zaitsev K. V. et al. Di-μ-oxido-bis(2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)] diphenolatotitanium(IV)) chloroform disolvate // Acta Crystallographica Section E Structure Reports Online. 2013. Vol. 69. No. 11. p. m626-m627.
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Zaitsev K. V., Karlov S. S., Zaitseva G. S., Lermontova E. K., Churakov A. V. Di-μ-oxido-bis(2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)] diphenolatotitanium(IV)) chloroform disolvate // Acta Crystallographica Section E Structure Reports Online. 2013. Vol. 69. No. 11. p. m626-m627.
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TY - JOUR
DO - 10.1107/S1600536813029371
UR - https://scripts.iucr.org/cgi-bin/paper?S1600536813029371
TI - Di-μ-oxido-bis(2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)] diphenolatotitanium(IV)) chloroform disolvate
T2 - Acta Crystallographica Section E Structure Reports Online
AU - Zaitsev, Kirill V.
AU - Karlov, Sergey S.
AU - Zaitseva, Galina S.
AU - Lermontova, Elmira Kh.
AU - Churakov, Andrei V.
PY - 2013
DA - 2013/10/31
PB - International Union of Crystallography (IUCr)
SP - m626-m627
IS - 11
VL - 69
PMID - 24454050
SN - 1600-5368
ER -
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@article{2013_Zaitsev,
author = {Kirill V. Zaitsev and Sergey S. Karlov and Galina S. Zaitseva and Elmira Kh. Lermontova and Andrei V. Churakov},
title = {Di-μ-oxido-bis(2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)] diphenolatotitanium(IV)) chloroform disolvate},
journal = {Acta Crystallographica Section E Structure Reports Online},
year = {2013},
volume = {69},
publisher = {International Union of Crystallography (IUCr)},
month = {oct},
url = {https://scripts.iucr.org/cgi-bin/paper?S1600536813029371},
number = {11},
pages = {m626--m627},
doi = {10.1107/S1600536813029371}
}
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Zaitsev, Kirill V., et al. “Di-μ-oxido-bis(2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)] diphenolatotitanium(IV)) chloroform disolvate.” Acta Crystallographica Section E Structure Reports Online, vol. 69, no. 11, Oct. 2013, pp. m626-m627. https://scripts.iucr.org/cgi-bin/paper?S1600536813029371.