Open Access
Journal of Synchrotron Radiation, volume 24, issue 1, pages 323-332
P13, the EMBL macromolecular crystallography beamline at the low-emittance PETRA III ring for high- and low-energy phasing with variable beam focusing
Cianci Michele
1
,
Bourenkov Gleb
1
,
Pompidor Guillaume
1
,
Karpics Ivars
1
,
Kallio Johanna
1
,
Bento Isabel
1
,
Roessle Manfred
1, 2
,
Cipriani Florent
3
,
Fiedler Stefan
1
,
1
Hamburg Unit c/o DESY, European Molecular Biology Laboratory (EMBL), Notkestrasse 85, 22603 Hamburg, Germany
|
2
Fachhochschule Lübeck, Fachbereich Angewandte Naturwissenschaften, Mönkhofer Weg 239, 23562 Lübeck, Germany
|
3
European Molecular Biology Laboratory, Institut Laue-Langevin, BP 181, 6 rue Jules Horowitz, 38042 Grenoble Cedex 9, France
|
Publication type: Journal Article
Publication date: 2017-01-01
Journal:
Journal of Synchrotron Radiation
Quartile SCImago
Q1
Quartile WOS
Q3
Impact factor: 2.5
ISSN: 09090495, 16005775
PubMed ID:
28009574
Instrumentation
Radiation
Nuclear and High Energy Physics
Abstract
The macromolecular crystallography P13 beamline is part of the European Molecular Biology Laboratory Integrated Facility for Structural Biology at PETRA III (DESY, Hamburg, Germany) and has been in user operation since mid-2013. P13 is tunable across the energy range from 4 to 17.5 keV to support crystallographic data acquisition exploiting a wide range of elemental absorption edges for experimental phase determination. An adaptive Kirkpatrick–Baez focusing system provides an X-ray beam with a high photon flux and tunable focus size to adapt to diverse experimental situations. Data collections at energies as low as 4 keV (λ = 3.1 Å) are possible due to a beamline design minimizing background and maximizing photon flux particularly at low energy (up to 1011 photons s−1 at 4 keV), a custom calibration of the PILATUS 6M-F detector for use at low energies, and the availability of a helium path. At high energies, the high photon flux (5.4 × 1011 photons s−1 at 17.5 keV) combined with a large area detector mounted on a 2θ arm allows data collection to sub-atomic resolution (0.55 Å). A peak flux of about 8.0 × 1012 photons s−1 is reached at 11 keV. Automated sample mounting is available by means of the robotic sample changer `MARVIN' with a dewar capacity of 160 samples. In close proximity to the beamline, laboratories have been set up for sample preparation and characterization; a laboratory specifically equipped for on-site heavy atom derivatization with a library of more than 150 compounds is available to beamline users.
Citations by journals
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IUCrJ
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1 publication, 0.67%
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1 publication, 0.67%
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Citations by publishers
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25
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Elsevier
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25 publications, 16.78%
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Wiley
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24 publications, 16.11%
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Springer Nature
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Royal Society of Chemistry (RSC)
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4 publications, 2.68%
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Frontiers Media S.A.
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3 publications, 2.01%
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Public Library of Science (PLoS)
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3 publications, 2.01%
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Taylor & Francis
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Taylor & Francis
2 publications, 1.34%
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Proceedings of the National Academy of Sciences (PNAS)
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Cold Spring Harbor Laboratory
1 publication, 0.67%
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5
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25
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- We do not take into account publications that without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Cianci M. et al. P13, the EMBL macromolecular crystallography beamline at the low-emittance PETRA III ring for high- and low-energy phasing with variable beam focusing // Journal of Synchrotron Radiation. 2017. Vol. 24. No. 1. pp. 323-332.
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Cianci M., Bourenkov G., Pompidor G., Karpics I., Kallio J., Bento I., Roessle M., Cipriani F., Fiedler S., Schneider T. P13, the EMBL macromolecular crystallography beamline at the low-emittance PETRA III ring for high- and low-energy phasing with variable beam focusing // Journal of Synchrotron Radiation. 2017. Vol. 24. No. 1. pp. 323-332.
Cite this
RIS
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TY - JOUR
DO - 10.1107/S1600577516016465
UR - https://doi.org/10.1107%2FS1600577516016465
TI - P13, the EMBL macromolecular crystallography beamline at the low-emittance PETRA III ring for high- and low-energy phasing with variable beam focusing
T2 - Journal of Synchrotron Radiation
AU - Bourenkov, Gleb
AU - Pompidor, Guillaume
AU - Karpics, Ivars
AU - Bento, Isabel
AU - Roessle, Manfred
AU - Cipriani, Florent
AU - Schneider, Thomas
AU - Fiedler, Stefan
AU - Cianci, Michele
AU - Kallio, Johanna
PY - 2017
DA - 2017/01/01 00:00:00
PB - Wiley
SP - 323-332
IS - 1
VL - 24
PMID - 28009574
SN - 0909-0495
SN - 1600-5775
ER -
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@article{2017_Cianci,
author = {Gleb Bourenkov and Guillaume Pompidor and Ivars Karpics and Isabel Bento and Manfred Roessle and Florent Cipriani and Thomas Schneider and Stefan Fiedler and Michele Cianci and Johanna Kallio},
title = {P13, the EMBL macromolecular crystallography beamline at the low-emittance PETRA III ring for high- and low-energy phasing with variable beam focusing},
journal = {Journal of Synchrotron Radiation},
year = {2017},
volume = {24},
publisher = {Wiley},
month = {jan},
url = {https://doi.org/10.1107%2FS1600577516016465},
number = {1},
pages = {323--332},
doi = {10.1107/S1600577516016465}
}
Cite this
MLA
Copy
Cianci, Michele, et al. “P13, the EMBL macromolecular crystallography beamline at the low-emittance PETRA III ring for high- and low-energy phasing with variable beam focusing.” Journal of Synchrotron Radiation, vol. 24, no. 1, Jan. 2017, pp. 323-332. https://doi.org/10.1107%2FS1600577516016465.
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