Low-Temperature Synthesis of Nanocrystalline Titanium Nitride via a Benzene-Thermal Route
Junqing Hu
1
,
Qingyi Lu
1
,
Kaibin Tang
1
,
Shu-Hong Yu
1
,
Y.L. Qian
1
,
GUIEN ZHOU
1
,
Xianming Liu
1
Publication type: Journal Article
Publication date: 2004-12-21
scimago Q1
wos Q1
SJR: 0.811
CiteScore: 7.2
Impact factor: 3.8
ISSN: 00027820, 15512916
Materials Chemistry
Ceramics and Composites
Abstract
A benzene–thermal reaction of TiCl4 and NaN3 at 350°–380°C was conducted for the preparation of nanocrystalline TiN. Powder X-ray diffractometry patterns indicated that the powder was cubic-phase TiN with a lattice constant a= 4.23656 A. Transmission electron microscopy images showed the TiN powders consisted of uniform spherical particles with an average diameter of 50 nm. The binding energies of Ti 2p3/2 and N 1s core levels at the positions of 454.85 and 397.1 eV, respectively, and the Ti:N atomic ratio of 1.08:1.00 were detected by X-ray photoelectron spectra. A possible formation mechanism of TiN was proposed.
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71
Total citations:
71
Citations from 2024:
5
(7.05%)
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MLA
Cite this
GOST
Copy
Hu J. et al. Low-Temperature Synthesis of Nanocrystalline Titanium Nitride via a Benzene-Thermal Route // Journal of the American Ceramic Society. 2004. Vol. 83. No. 2. pp. 430-432.
GOST all authors (up to 50)
Copy
Hu J., Lu Q., Tang K., Yu S., Qian Y., ZHOU G., Liu X. Low-Temperature Synthesis of Nanocrystalline Titanium Nitride via a Benzene-Thermal Route // Journal of the American Ceramic Society. 2004. Vol. 83. No. 2. pp. 430-432.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1111/j.1151-2916.2000.tb01212.x
UR - https://doi.org/10.1111/j.1151-2916.2000.tb01212.x
TI - Low-Temperature Synthesis of Nanocrystalline Titanium Nitride via a Benzene-Thermal Route
T2 - Journal of the American Ceramic Society
AU - Hu, Junqing
AU - Lu, Qingyi
AU - Tang, Kaibin
AU - Yu, Shu-Hong
AU - Qian, Y.L.
AU - ZHOU, GUIEN
AU - Liu, Xianming
PY - 2004
DA - 2004/12/21
PB - Wiley
SP - 430-432
IS - 2
VL - 83
SN - 0002-7820
SN - 1551-2916
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2004_Hu,
author = {Junqing Hu and Qingyi Lu and Kaibin Tang and Shu-Hong Yu and Y.L. Qian and GUIEN ZHOU and Xianming Liu},
title = {Low-Temperature Synthesis of Nanocrystalline Titanium Nitride via a Benzene-Thermal Route},
journal = {Journal of the American Ceramic Society},
year = {2004},
volume = {83},
publisher = {Wiley},
month = {dec},
url = {https://doi.org/10.1111/j.1151-2916.2000.tb01212.x},
number = {2},
pages = {430--432},
doi = {10.1111/j.1151-2916.2000.tb01212.x}
}
Cite this
MLA
Copy
Hu, Junqing, et al. “Low-Temperature Synthesis of Nanocrystalline Titanium Nitride via a Benzene-Thermal Route.” Journal of the American Ceramic Society, vol. 83, no. 2, Dec. 2004, pp. 430-432. https://doi.org/10.1111/j.1151-2916.2000.tb01212.x.