Pleiades Publishing
Russian Journal of Inorganic Chemistry
,  volume 66 ,  issue 7 ,  pages 963-968

Synthesis and Deep Purification of Tin Tetrachloride

Publication type: Journal Article
Publication date: 2021-07-12
Pleiades Publishing
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
The results of development of physicochemical fundamentals for the synthesis and deep purification of tin tetrachloride have been described. The samples of SnCl4 have been prepared from elements in a specially designed quartz installation. Prepared SnCl4 has been purified by rectification on a perforated-plate column. It has been revealed by mass spectrometry that the content of lead admixture after SnCl4 rectification decreases from 120 to 2 ppm, and the content of admixtures of other metals decreases considerably. Separation factors in liquid–vapor system for hardly separable admixtures have been calculated. The purity of SnCl4 samples has been confirmed by IR and Raman spectroscopy. The prepared SnCl4 samples contained 10–4 wt % of admixtures.
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GOST |
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GOST Copy
Mastryukov M. V. et al. Synthesis and Deep Purification of Tin Tetrachloride // Russian Journal of Inorganic Chemistry. 2021. Vol. 66. No. 7. pp. 963-968.
GOST all authors (up to 50) Copy
Mastryukov M. V., Demina L. I., Moiseeva L., Soldatkina A. D., Brekhovskikh M. N. Synthesis and Deep Purification of Tin Tetrachloride // Russian Journal of Inorganic Chemistry. 2021. Vol. 66. No. 7. pp. 963-968.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1134/S003602362107007X
UR - https://doi.org/10.1134/S003602362107007X
TI - Synthesis and Deep Purification of Tin Tetrachloride
T2 - Russian Journal of Inorganic Chemistry
AU - Mastryukov, M V
AU - Demina, L. I.
AU - Moiseeva, L.V.
AU - Soldatkina, A D
AU - Brekhovskikh, M N
PY - 2021
DA - 2021/07/12
PB - Pleiades Publishing
SP - 963-968
IS - 7
VL - 66
SN - 0036-0236
SN - 1531-8613
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2021_Mastryukov,
author = {M V Mastryukov and L. I. Demina and L.V. Moiseeva and A D Soldatkina and M N Brekhovskikh},
title = {Synthesis and Deep Purification of Tin Tetrachloride},
journal = {Russian Journal of Inorganic Chemistry},
year = {2021},
volume = {66},
publisher = {Pleiades Publishing},
month = {jul},
url = {https://doi.org/10.1134/S003602362107007X},
number = {7},
pages = {963--968},
doi = {10.1134/S003602362107007X}
}
MLA
Cite this
MLA Copy
Mastryukov, M. V., et al. “Synthesis and Deep Purification of Tin Tetrachloride.” Russian Journal of Inorganic Chemistry, vol. 66, no. 7, Jul. 2021, pp. 963-968. https://doi.org/10.1134/S003602362107007X.