Synthesis and Deep Purification of Tin Tetrachloride
Тип публикации: Journal Article
Дата публикации: 2021-07-12
scimago Q3
wos Q4
БС2
SJR: 0.27
CiteScore: 3
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Краткое описание
The results of development of physicochemical fundamentals for the synthesis and deep purification of tin tetrachloride have been described. The samples of SnCl4 have been prepared from elements in a specially designed quartz installation. Prepared SnCl4 has been purified by rectification on a perforated-plate column. It has been revealed by mass spectrometry that the content of lead admixture after SnCl4 rectification decreases from 120 to 2 ppm, and the content of admixtures of other metals decreases considerably. Separation factors in liquid–vapor system for hardly separable admixtures have been calculated. The purity of SnCl4 samples has been confirmed by IR and Raman spectroscopy. The prepared SnCl4 samples contained 10–4 wt % of admixtures.
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Russian Journal of Inorganic Chemistry
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Mendeleev Communications
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Inorganic Materials
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Pleiades Publishing
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Elsevier
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Mastryukov M. V. et al. Synthesis and Deep Purification of Tin Tetrachloride // Russian Journal of Inorganic Chemistry. 2021. Vol. 66. No. 7. pp. 963-968.
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Mastryukov M. V., Demina L. I., Moiseeva L., Soldatkina A. D., Brekhovskikh M. N. Synthesis and Deep Purification of Tin Tetrachloride // Russian Journal of Inorganic Chemistry. 2021. Vol. 66. No. 7. pp. 963-968.
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TY - JOUR
DO - 10.1134/S003602362107007X
UR - https://doi.org/10.1134/S003602362107007X
TI - Synthesis and Deep Purification of Tin Tetrachloride
T2 - Russian Journal of Inorganic Chemistry
AU - Mastryukov, M V
AU - Demina, L. I.
AU - Moiseeva, L.V.
AU - Soldatkina, A D
AU - Brekhovskikh, M N
PY - 2021
DA - 2021/07/12
PB - Pleiades Publishing
SP - 963-968
IS - 7
VL - 66
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2021_Mastryukov,
author = {M V Mastryukov and L. I. Demina and L.V. Moiseeva and A D Soldatkina and M N Brekhovskikh},
title = {Synthesis and Deep Purification of Tin Tetrachloride},
journal = {Russian Journal of Inorganic Chemistry},
year = {2021},
volume = {66},
publisher = {Pleiades Publishing},
month = {jul},
url = {https://doi.org/10.1134/S003602362107007X},
number = {7},
pages = {963--968},
doi = {10.1134/S003602362107007X}
}
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MLA
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Mastryukov, M. V., et al. “Synthesis and Deep Purification of Tin Tetrachloride.” Russian Journal of Inorganic Chemistry, vol. 66, no. 7, Jul. 2021, pp. 963-968. https://doi.org/10.1134/S003602362107007X.