Structures of Acylated 5-Iodo-8-Hydroxyquinoline and 5,7-Diiodo-8-Hydroxyquinoline Derivatives
Publication type: Journal Article
Publication date: 2025-03-29
scimago Q4
wos Q4
SJR: 0.211
CiteScore: 1.9
Impact factor: 1.4
ISSN: 00224766, 15738779
Abstract
The 5-I-8-HqAc (1) and 5,7-I2-8-HqAc (2) acyl derivatives are prepared by the interaction of 5-iodo-8-hydroxyquinoline (5-I-8-Hq) and 5,7-diiodo-8-hydroxyquinoline (5,7-I2-8-HqAc) with acetic anhydride at 80 °C. Crystals of these compounds are obtained by the recrystallization from chloroform. The crystal structures of 1 and 2 are determined by XRD, the revealed structural features are discussed. The intermolecular contacts influencing the crystal packing are analyzed; Hirshfeld surfaces are constructed. It is shown that the monoiodide contains short I⋯N halogen bonds, whereas the diiodide contains only short I⋯I contacts.
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Senchurin V. S. et al. Structures of Acylated 5-Iodo-8-Hydroxyquinoline and 5,7-Diiodo-8-Hydroxyquinoline Derivatives // Journal of Structural Chemistry. 2025. Vol. 66. No. 3. pp. 595-602.
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Senchurin V. S., Nayfert S. A., Osipov A. A., Zherebtsov D. A., Kantkhapazham R. Structures of Acylated 5-Iodo-8-Hydroxyquinoline and 5,7-Diiodo-8-Hydroxyquinoline Derivatives // Journal of Structural Chemistry. 2025. Vol. 66. No. 3. pp. 595-602.
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TY - JOUR
DO - 10.1134/s0022476625030151
UR - https://link.springer.com/10.1134/S0022476625030151
TI - Structures of Acylated 5-Iodo-8-Hydroxyquinoline and 5,7-Diiodo-8-Hydroxyquinoline Derivatives
T2 - Journal of Structural Chemistry
AU - Senchurin, V S
AU - Nayfert, S. A.
AU - Osipov, A. A.
AU - Zherebtsov, D. A.
AU - Kantkhapazham, R.
PY - 2025
DA - 2025/03/29
PB - Pleiades Publishing
SP - 595-602
IS - 3
VL - 66
SN - 0022-4766
SN - 1573-8779
ER -
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@article{2025_Senchurin,
author = {V S Senchurin and S. A. Nayfert and A. A. Osipov and D. A. Zherebtsov and R. Kantkhapazham},
title = {Structures of Acylated 5-Iodo-8-Hydroxyquinoline and 5,7-Diiodo-8-Hydroxyquinoline Derivatives},
journal = {Journal of Structural Chemistry},
year = {2025},
volume = {66},
publisher = {Pleiades Publishing},
month = {mar},
url = {https://link.springer.com/10.1134/S0022476625030151},
number = {3},
pages = {595--602},
doi = {10.1134/s0022476625030151}
}
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MLA
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Senchurin, V. S., et al. “Structures of Acylated 5-Iodo-8-Hydroxyquinoline and 5,7-Diiodo-8-Hydroxyquinoline Derivatives.” Journal of Structural Chemistry, vol. 66, no. 3, Mar. 2025, pp. 595-602. https://link.springer.com/10.1134/S0022476625030151.