Conversions of zinc cimantrenates in reactions with 1,10-phenanthroline
Publication type: Journal Article
Publication date: 2015-09-27
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
The reaction between aqueous zinc acetate and cimantrene carboxylic acid has been found to yield Zn[(OOCC5H4)Mn(CO)3] 2[O(H)Me]4, whose dissolution in tetrahydrofuran (THF) gives trinuclear Zn3[μ-(OOCC5H4)Mn(CO)3]4[μ-η2-(OOCC5H4)Mn(CO)3]2(THF)4. Labile THF molecules can be replaced by bidentate 1,10-phenanthroline under mild conditions, thus resulting in Phen2Zn3[μ-(OOCC5H4)Mn(CO)3]4[μ-η2- (OOCC5H4)Mn(CO)3]2. Variations in the reagent ratio and the reaction conditions result in mononuclear PhenZn[(OOCC5H4)Mn(CO)3]2(H2O), which contains a coordinated water molecule. The synthesized complexes have been separated with high yields in the form of single crystals and characterized by chemical analysis, IR spectroscopy, and X-ray diffraction.
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Uvarova M. A., Ageshina A. A., Nefedov S. Conversions of zinc cimantrenates in reactions with 1,10-phenanthroline // Russian Journal of Inorganic Chemistry. 2015. Vol. 60. No. 10. pp. 1210-1217.
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Uvarova M. A., Ageshina A. A., Nefedov S. Conversions of zinc cimantrenates in reactions with 1,10-phenanthroline // Russian Journal of Inorganic Chemistry. 2015. Vol. 60. No. 10. pp. 1210-1217.
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RIS
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TY - JOUR
DO - 10.1134/s0036023615100198
UR - https://doi.org/10.1134/s0036023615100198
TI - Conversions of zinc cimantrenates in reactions with 1,10-phenanthroline
T2 - Russian Journal of Inorganic Chemistry
AU - Uvarova, M A
AU - Ageshina, A A
AU - Nefedov, S.E.
PY - 2015
DA - 2015/09/27
PB - Pleiades Publishing
SP - 1210-1217
IS - 10
VL - 60
SN - 0036-0236
SN - 1531-8613
ER -
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BibTex (up to 50 authors)
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@article{2015_Uvarova,
author = {M A Uvarova and A A Ageshina and S.E. Nefedov},
title = {Conversions of zinc cimantrenates in reactions with 1,10-phenanthroline},
journal = {Russian Journal of Inorganic Chemistry},
year = {2015},
volume = {60},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://doi.org/10.1134/s0036023615100198},
number = {10},
pages = {1210--1217},
doi = {10.1134/s0036023615100198}
}
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Uvarova, M. A., et al. “Conversions of zinc cimantrenates in reactions with 1,10-phenanthroline.” Russian Journal of Inorganic Chemistry, vol. 60, no. 10, Sep. 2015, pp. 1210-1217. https://doi.org/10.1134/s0036023615100198.
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