Synthesis and Structure of Cyclometallated Palladium Binuclear Complexes with Bridging Carboxylate Ligands
J. E. Makarevich
1
,
N. K. Ogarkova
1
,
E A Sosunov
1
,
O. V. Sulimova
1
,
I V Skabitsky
1
,
A S Popova
1
,
M V Panina
1
,
M Yu Nesterenko
1
,
M.N. Vargaftik
1
,
Publication type: Journal Article
Publication date: 2023-09-01
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
New bimetallic pivalate Pd(II) complex [PdNi(OOCtBu)4(HOOCtBu)] (I) has been synthesized from [PdNi(OOCMe)4] and used as a starting reagent in a further complexation reaction. Cyclometallated binuclear carboxylate palladium complexes [(OOCMe)Pd(2‑phpy)]2 (II) and [(OOCtBu)Pd(2‑phpy)]2 (III) have been obtained by the reaction between heterometallic compounds [Pd(OOCR)4Ni] (R = Me, tBu) and 2-phenylpyridine (2-phpy). The reaction proceeds at room temperature under mild conditions. All the compounds obtained have been isolated in crystalline form from a medium of nonpolar solvents, characterized by single-crystal X-ray diffraction analysis, and deposited at the Cambridge Crystallographic Data Center (CCDC nos. 2256606 for I, 2247942 for II, and 2247943 for III).
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Makarevich J. E. et al. Synthesis and Structure of Cyclometallated Palladium Binuclear Complexes with Bridging Carboxylate Ligands // Russian Journal of Inorganic Chemistry. 2023. Vol. 68. No. 9. pp. 1217-1227.
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Makarevich J. E., Ogarkova N. K., Sosunov E. A., Sulimova O. V., Skabitsky I. V., Popova A. S., Panina M. V., Nesterenko M. Yu., Vargaftik M., Yakushev I. A. Synthesis and Structure of Cyclometallated Palladium Binuclear Complexes with Bridging Carboxylate Ligands // Russian Journal of Inorganic Chemistry. 2023. Vol. 68. No. 9. pp. 1217-1227.
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RIS
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TY - JOUR
DO - 10.1134/s0036023623601708
UR - https://link.springer.com/10.1134/S0036023623601708
TI - Synthesis and Structure of Cyclometallated Palladium Binuclear Complexes with Bridging Carboxylate Ligands
T2 - Russian Journal of Inorganic Chemistry
AU - Makarevich, J. E.
AU - Ogarkova, N. K.
AU - Sosunov, E A
AU - Sulimova, O. V.
AU - Skabitsky, I V
AU - Popova, A S
AU - Panina, M V
AU - Nesterenko, M Yu
AU - Vargaftik, M.N.
AU - Yakushev, I A
PY - 2023
DA - 2023/09/01
PB - Pleiades Publishing
SP - 1217-1227
IS - 9
VL - 68
SN - 0036-0236
SN - 1531-8613
ER -
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BibTex (up to 50 authors)
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@article{2023_Makarevich,
author = {J. E. Makarevich and N. K. Ogarkova and E A Sosunov and O. V. Sulimova and I V Skabitsky and A S Popova and M V Panina and M Yu Nesterenko and M.N. Vargaftik and I A Yakushev},
title = {Synthesis and Structure of Cyclometallated Palladium Binuclear Complexes with Bridging Carboxylate Ligands},
journal = {Russian Journal of Inorganic Chemistry},
year = {2023},
volume = {68},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://link.springer.com/10.1134/S0036023623601708},
number = {9},
pages = {1217--1227},
doi = {10.1134/s0036023623601708}
}
Cite this
MLA
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Makarevich, J. E., et al. “Synthesis and Structure of Cyclometallated Palladium Binuclear Complexes with Bridging Carboxylate Ligands.” Russian Journal of Inorganic Chemistry, vol. 68, no. 9, Sep. 2023, pp. 1217-1227. https://link.springer.com/10.1134/S0036023623601708.