Russian Journal of Physical Chemistry A, volume 98, issue 13, pages 3220-3226

Studying the Electrochemical Behavior of a Smooth Gold Electrode in a Solution of Bridged 1,2,4-Trioxalane in Acetonitrile

M.V. Polyakov ¹

M D Vedenyapina ¹

A M Skundin ²

I A Yaremenko ¹

P S Radulov ¹

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Zelinsky Institute of Organic chemistry, Russian Academy of Sciences, Moscow, Russia |

Frumkin Institute of Physical Chemistry and electrochemistry, Russian Academy of Sciences, Moscow, Russia |

Publication type: Journal Article

Publication date: 2024-12-01

Pleiades Publishing

Journal: Russian Journal of Physical Chemistry A

scimago Q4

wos Q4

SJR: 0.198

CiteScore: 1.2

Impact factor: 0.7

ISSN: 00360244, 1531863X

DOI: 10.1134/s0036024424702443

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Abstract

Cyclic voltammetry and gravimetry are used to study the behavior of a smooth gold electrode in a medium of bridged 1,2,4-trioxalane in acetonitrile. It is found that the peroxide bond in the molecule of bridged 1,2,4-trioxalane is reduced on the surface of the electrode during the cathodic process, with the subsequent formation of a diketone fragment. The formation of colloidal gold particles is detected during anodic oxidation.

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Publisher

Pleiades Publishing

Journal

Russian Journal of Physical Chemistry A

scimago Q4

wos Q4

SJR

0.198

CiteScore

1.2

Impact factor

0.7

ISSN

00360244 (Print)

1531863X (Electronic)