,
volume 37
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issue 10
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pages 781-784
Tris(2-methoxy-5-bromophenyl)antimony bis(2-nitrobenzoate): Synthesis and specific features of the structure
1
Blagoveshchensk State Pedagogical University, Blagoveshchensk, Russia
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Publication type: Journal Article
Publication date: 2011-10-05
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
Tris(5-bromo-2-methoxyphenyl)antimony bis(2-nitrobenzoate) (I) is synthesized by the reaction of tris(5-bromo-2-methoxyphenyl)antimony with 2-nitrobenzoic acid in the presence of hydrogen peroxide (mole ratio 1: 2: 1). According to the X-ray diffraction data, the antimony atom has distorted trigonal bipyramidal coordination. The axial angle OSbO is 177.92(11)°, equatorial bonds CSbC are 109.23(16)°–128.31(16)°, and the Sb-O and Sb-C bond lengths are 2.095(3)–2.125(3) and 2.098(4)–2.113(4) Å, respectively. A specific feature of the structure of complex I is the presence of intramolecular contacts Sb...O(CH3) (2.992–3.175 Å along with the interactions Sb...O=C (3.039–3.117 Å). The structural organization in crystal is due to weak hydrogen bonds N-O...H-C, C=O...H-C, C-Br...H-C.
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Sharutin V. V. et al. Tris(2-methoxy-5-bromophenyl)antimony bis(2-nitrobenzoate): Synthesis and specific features of the structure // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2011. Vol. 37. No. 10. pp. 781-784.
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Sharutin V. V., Senchurin V. S., Sharutina O. K., Chagarova O. V., Zelevets L. E. Tris(2-methoxy-5-bromophenyl)antimony bis(2-nitrobenzoate): Synthesis and specific features of the structure // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2011. Vol. 37. No. 10. pp. 781-784.
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TY - JOUR
DO - 10.1134/s1070328411090089
UR - https://doi.org/10.1134/s1070328411090089
TI - Tris(2-methoxy-5-bromophenyl)antimony bis(2-nitrobenzoate): Synthesis and specific features of the structure
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Sharutin, V V
AU - Senchurin, V S
AU - Sharutina, O K
AU - Chagarova, O V
AU - Zelevets, L E
PY - 2011
DA - 2011/10/05
PB - Pleiades Publishing
SP - 781-784
IS - 10
VL - 37
SN - 1070-3284
SN - 1608-3318
ER -
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@article{2011_Sharutin,
author = {V V Sharutin and V S Senchurin and O K Sharutina and O V Chagarova and L E Zelevets},
title = {Tris(2-methoxy-5-bromophenyl)antimony bis(2-nitrobenzoate): Synthesis and specific features of the structure},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2011},
volume = {37},
publisher = {Pleiades Publishing},
month = {oct},
url = {https://doi.org/10.1134/s1070328411090089},
number = {10},
pages = {781--784},
doi = {10.1134/s1070328411090089}
}
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MLA
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Sharutin, V. V., et al. “Tris(2-methoxy-5-bromophenyl)antimony bis(2-nitrobenzoate): Synthesis and specific features of the structure.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 37, no. 10, Oct. 2011, pp. 781-784. https://doi.org/10.1134/s1070328411090089.