Efficient synthetic methods for unsaturated 3,4,5-trimethoxybenzyl sulfides and ethers
Publication type: Journal Article
Publication date: 2016-11-01
scimago Q4
wos Q4
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Organic Chemistry
Abstract
Convenient and efficient procedures were developed for preparation of 3,4,5-trimethoxybenzyl sulfides and ethers containing vinyl, allyl, and propargyl groups proceeding from 3,4,5-trimethoxybenzyl alcohol, elemental sulfur, and thiourea in basic and basic-reductive systems (hydrazine hydrate‒KОН‒DMF, NaBH4‒EtOH, KОН‒DMSO). The effective method of the synthesis of 1,1'-[disulfandiylbis(methylene)]bis-(3,4,5-trimethoxybenzene) consists in the reduction of the elemental sulfur to disulfide anion with hydrazine hydrate in the presence of KОН followed by the reaction with 3,4,5-trimethoxybenzyl chloride under the conditions of phase-transfer catalysis or in DMF.
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Potapov V. A. et al. Efficient synthetic methods for unsaturated 3,4,5-trimethoxybenzyl sulfides and ethers // Russian Journal of Organic Chemistry. 2016. Vol. 52. No. 11. pp. 1571-1575.
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Potapov V. A., Panov V., Musalov M. V., Zhiveteva S. A., Musalova M. V., Khabibulina A. G., Amosova S. V. Efficient synthetic methods for unsaturated 3,4,5-trimethoxybenzyl sulfides and ethers // Russian Journal of Organic Chemistry. 2016. Vol. 52. No. 11. pp. 1571-1575.
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TY - JOUR
DO - 10.1134/s107042801611004x
UR - https://doi.org/10.1134/s107042801611004x
TI - Efficient synthetic methods for unsaturated 3,4,5-trimethoxybenzyl sulfides and ethers
T2 - Russian Journal of Organic Chemistry
AU - Potapov, V. A.
AU - Panov, V.A
AU - Musalov, M V
AU - Zhiveteva, S A
AU - Musalova, M V
AU - Khabibulina, A G
AU - Amosova, S V
PY - 2016
DA - 2016/11/01
PB - Pleiades Publishing
SP - 1571-1575
IS - 11
VL - 52
SN - 1070-4280
SN - 1608-3393
ER -
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@article{2016_Potapov,
author = {V. A. Potapov and V.A Panov and M V Musalov and S A Zhiveteva and M V Musalova and A G Khabibulina and S V Amosova},
title = {Efficient synthetic methods for unsaturated 3,4,5-trimethoxybenzyl sulfides and ethers},
journal = {Russian Journal of Organic Chemistry},
year = {2016},
volume = {52},
publisher = {Pleiades Publishing},
month = {nov},
url = {https://doi.org/10.1134/s107042801611004x},
number = {11},
pages = {1571--1575},
doi = {10.1134/s107042801611004x}
}
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MLA
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Potapov, V. A., et al. “Efficient synthetic methods for unsaturated 3,4,5-trimethoxybenzyl sulfides and ethers.” Russian Journal of Organic Chemistry, vol. 52, no. 11, Nov. 2016, pp. 1571-1575. https://doi.org/10.1134/s107042801611004x.