Insertion of ethyl isothiocyanate into tungsten hexachloride: Crystal structure of ethyl-(4-ethyl-5-thioxo[1.2.4]dithiazolidin-3-ylidene)ammonium oxopentachlorotungstate(VI)
Тип публикации: Journal Article
Дата публикации: 2003-07-01
scimago Q4
wos Q4
БС2
SJR: 0.145
CiteScore: 0.8
Impact factor: 0.5
ISSN: 10637745, 1562689X
General Chemistry
Condensed Matter Physics
General Materials Science
Краткое описание
A product of the insertion of two isothiocyanate molecules into the same W-Cl bond, namely, W-Cl-WCl5{N(Et)C(S)N(Et)C(S)Cl} (I), is synthesized by the reaction of WCl6 with EtNCS in a dichloroethane solution. The hydrolysis of compound I results in the formation of single crystals of the complex . The structure of crystals II is determined using X-ray diffraction. It is demonstrated that structural units of crystals II are the [WVIOCl5]− anionic complexes and the ethyl-(4-ethyl-5-thioxo[1.2.4]dithiazolidin-3-ylidene)ammonium cations.
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Ovchinnikova N. et al. Insertion of ethyl isothiocyanate into tungsten hexachloride: Crystal structure of ethyl-(4-ethyl-5-thioxo[1.2.4]dithiazolidin-3-ylidene)ammonium oxopentachlorotungstate(VI) // Crystallography Reports. 2003. Vol. 48. No. 4. pp. 602-605.
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Ovchinnikova N., Sinyakov A. E., Sergienko V. S., Aleksandrov G. Insertion of ethyl isothiocyanate into tungsten hexachloride: Crystal structure of ethyl-(4-ethyl-5-thioxo[1.2.4]dithiazolidin-3-ylidene)ammonium oxopentachlorotungstate(VI) // Crystallography Reports. 2003. Vol. 48. No. 4. pp. 602-605.
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TY - JOUR
DO - 10.1134/1.1595186
UR - https://doi.org/10.1134/1.1595186
TI - Insertion of ethyl isothiocyanate into tungsten hexachloride: Crystal structure of ethyl-(4-ethyl-5-thioxo[1.2.4]dithiazolidin-3-ylidene)ammonium oxopentachlorotungstate(VI)
T2 - Crystallography Reports
AU - Ovchinnikova, N.A.
AU - Sinyakov, A E
AU - Sergienko, V S
AU - Aleksandrov, G.G.
PY - 2003
DA - 2003/07/01
PB - Pleiades Publishing
SP - 602-605
IS - 4
VL - 48
SN - 1063-7745
SN - 1562-689X
ER -
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@article{2003_Ovchinnikova,
author = {N.A. Ovchinnikova and A E Sinyakov and V S Sergienko and G.G. Aleksandrov},
title = {Insertion of ethyl isothiocyanate into tungsten hexachloride: Crystal structure of ethyl-(4-ethyl-5-thioxo[1.2.4]dithiazolidin-3-ylidene)ammonium oxopentachlorotungstate(VI)},
journal = {Crystallography Reports},
year = {2003},
volume = {48},
publisher = {Pleiades Publishing},
month = {jul},
url = {https://doi.org/10.1134/1.1595186},
number = {4},
pages = {602--605},
doi = {10.1134/1.1595186}
}
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Ovchinnikova, N.A., et al. “Insertion of ethyl isothiocyanate into tungsten hexachloride: Crystal structure of ethyl-(4-ethyl-5-thioxo[1.2.4]dithiazolidin-3-ylidene)ammonium oxopentachlorotungstate(VI).” Crystallography Reports, vol. 48, no. 4, Jul. 2003, pp. 602-605. https://doi.org/10.1134/1.1595186.