Doklady Physical Chemistry

, volume 491 , issue 2 , pages 40-42

Identification of the Structure of Polybutadiene Terminal Units by NMR Spectroscopy with T 2-Filter

V A Rozentsvet ¹

N A Sablina ¹

D M Ulyanova ¹

P M Tolstoy ²

S. N. Smirnov ²

I A Novakov ³

Hide authors affiliations Show authors affiliations: 3 affiliations

Institute of Ecology of the Volga River Basin, Samara Federal Research Center, Russian Academy of Sciences, Togliatti, Russia

Institute of Ecology of Volga River Basin RAS

Samara Federal Research Center of the Russian Academy of Sciences

St. Petersburg state University, St. Petersburg, Russia |

Volgograd State technical University, Volgograd, Russia |

Publication type: Journal Article

Publication date: 2020-04-01

Pleiades Publishing

Doklady Physical Chemistry

scimago Q4

wos Q4

SJR: 0.195

CiteScore: 1.7

Impact factor: 1.5

ISSN: 00125016, 16083121

DOI: 10.1134/S0012501620040028

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Physical and Theoretical Chemistry

Abstract

A new method for the identification of the structure of terminal units in polybutadiene synthesized by cationic polymerization has been developed. The method consists of conducting T2-filtered NMR experiments, which make it possible to reduce the intensities of the spectral signals of the main-chain carbon atoms and significantly increase the intensities of the signals of the carbon atoms in the head and end polybutadiene units characterized by higher mobility.

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Rozentsvet V. A. et al. Identification of the Structure of Polybutadiene Terminal Units by NMR Spectroscopy with T 2-Filter // Doklady Physical Chemistry. 2020. Vol. 491. No. 2. pp. 40-42.

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Rozentsvet V. A., Sablina N. A., Ulyanova D. M., Tolstoy P. M., Smirnov S. N., Novakov I. A. Identification of the Structure of Polybutadiene Terminal Units by NMR Spectroscopy with T 2-Filter // Doklady Physical Chemistry. 2020. Vol. 491. No. 2. pp. 40-42.

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RIS Copy

TY - JOUR

DO - 10.1134/S0012501620040028

UR - https://doi.org/10.1134/S0012501620040028

TI - Identification of the Structure of Polybutadiene Terminal Units by NMR Spectroscopy with T 2-Filter

T2 - Doklady Physical Chemistry

AU - Rozentsvet, V A

AU - Sablina, N A

AU - Ulyanova, D M

AU - Tolstoy, P M

AU - Smirnov, S. N.

AU - Novakov, I A

PY - 2020

DA - 2020/04/01

PB - Pleiades Publishing

SP - 40-42

IS - 2

VL - 491

SN - 0012-5016

SN - 1608-3121

ER -

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@article{2020_Rozentsvet,

author = {V A Rozentsvet and N A Sablina and D M Ulyanova and P M Tolstoy and S. N. Smirnov and I A Novakov},

title = {Identification of the Structure of Polybutadiene Terminal Units by NMR Spectroscopy with T 2-Filter},

journal = {Doklady Physical Chemistry},

year = {2020},

volume = {491},

publisher = {Pleiades Publishing},

month = {apr},

url = {https://doi.org/10.1134/S0012501620040028},

number = {2},

pages = {40--42},

doi = {10.1134/S0012501620040028}

}

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Rozentsvet, V. A., et al. “Identification of the Structure of Polybutadiene Terminal Units by NMR Spectroscopy with T 2-Filter.” Doklady Physical Chemistry, vol. 491, no. 2, Apr. 2020, pp. 40-42. https://doi.org/10.1134/S0012501620040028.