Pleiades Publishing
Inorganic Materials
,  volume 55 ,  issue 9 ,  pages 974-978

Synthesis and Ultrapurification of Tin Diiodide

M N Brekhovskikh 1
, 
M V Mastryukov 1
, 
P V Kornev 2
, 
A A Gasanov 2
, 
A E Kovalenko 3
, 
V.A. Fedorov 1
1
 
2
 
3
 
Specialty Chemistry Research Center, Moscow, Russia | 
Publication type: Journal Article
Publication date: 2019-09-16
Pleiades Publishing
scimago Q4
wos Q4
SJR: 0.183
CiteScore: 1.3
Impact factor: 0.7
ISSN: 00201685, 16083172
Materials Chemistry
Metals and Alloys
Inorganic Chemistry
General Chemical Engineering
Abstract
This paper presents results of a study aimed at developing physicochemical principles of tin diiodide (SnI2) synthesis and ultrapurification by high-temperature fractional distillation. SnI2 samples were synthesized by different processes: in solution, from elemental mixtures at atmospheric pressure, and in a vacuum. Next, the samples were purified by fractional distillation in a plate column. Separation factors of difficult-to-remove impurities in the SnI2-based liquid–vapor system have been determined experimentally. We have prepared and characterized extrapure-grade SnI2 containing 10 ppm by weight of trace impurities
Found 
Found 

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GOST |
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GOST Copy
Brekhovskikh M. N. et al. Synthesis and Ultrapurification of Tin Diiodide // Inorganic Materials. 2019. Vol. 55. No. 9. pp. 974-978.
GOST all authors (up to 50) Copy
Brekhovskikh M. N., Mastryukov M. V., Kornev P. V., Gasanov A. A., Kovalenko A. E., Fedorov V. Synthesis and Ultrapurification of Tin Diiodide // Inorganic Materials. 2019. Vol. 55. No. 9. pp. 974-978.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1134/S0020168519090012
UR - https://doi.org/10.1134/S0020168519090012
TI - Synthesis and Ultrapurification of Tin Diiodide
T2 - Inorganic Materials
AU - Brekhovskikh, M N
AU - Mastryukov, M V
AU - Kornev, P V
AU - Gasanov, A A
AU - Kovalenko, A E
AU - Fedorov, V.A.
PY - 2019
DA - 2019/09/16
PB - Pleiades Publishing
SP - 974-978
IS - 9
VL - 55
SN - 0020-1685
SN - 1608-3172
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2019_Brekhovskikh,
author = {M N Brekhovskikh and M V Mastryukov and P V Kornev and A A Gasanov and A E Kovalenko and V.A. Fedorov},
title = {Synthesis and Ultrapurification of Tin Diiodide},
journal = {Inorganic Materials},
year = {2019},
volume = {55},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://doi.org/10.1134/S0020168519090012},
number = {9},
pages = {974--978},
doi = {10.1134/S0020168519090012}
}
MLA
Cite this
MLA Copy
Brekhovskikh, M. N., et al. “Synthesis and Ultrapurification of Tin Diiodide.” Inorganic Materials, vol. 55, no. 9, Sep. 2019, pp. 974-978. https://doi.org/10.1134/S0020168519090012.