Crystal structure and thermal properties of [Au(en)2]2[Cu(C2O4)2]3·8H2O
E V Makotchenko
1, 2
,
E A Bykova
1
,
E Yu Semitut
1, 2
,
Yu. V. Shubin
1, 2
,
P V Snytnikov
2, 3
,
P E Plyusnin
1, 2
Publication type: Journal Article
Publication date: 2011-10-01
scimago Q4
wos Q4
SJR: 0.211
CiteScore: 1.9
Impact factor: 1.4
ISSN: 00224766, 15738779
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
The crystal structure of a double complex salt of the composition [Au(en)2]2[Cu(C2O4)2]3·8H2O (en = ethylenediamine) at 150 K is determined by single crystal X-ray diffraction. The crystal data for C20H48Au2Cu3N8O32 are: a = 9.1761(3) Å, b = 16.9749(6) Å, c = 13.4475(5) Å, β = 104.333(1)°, V = 2029.43(12) Å3, P21/c space group, Z = 2, d x = 2.450 g/cm3. It is demonstrated that the thermal decomposition of the double complex salt in a helium or hydrogen atmosphere affords the solid solution Au0.4Cu0.6.
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Makotchenko E. V. et al. Crystal structure and thermal properties of [Au(en)2]2[Cu(C2O4)2]3·8H2O // Journal of Structural Chemistry. 2011. Vol. 52. No. 5. pp. 924-929.
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Makotchenko E. V., Bykova E. A., Semitut E. Yu., Shubin Y. V., Snytnikov P. V., Plyusnin P. E. Crystal structure and thermal properties of [Au(en)2]2[Cu(C2O4)2]3·8H2O // Journal of Structural Chemistry. 2011. Vol. 52. No. 5. pp. 924-929.
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TY - JOUR
DO - 10.1134/S002247661105012X
UR - https://doi.org/10.1134/S002247661105012X
TI - Crystal structure and thermal properties of [Au(en)2]2[Cu(C2O4)2]3·8H2O
T2 - Journal of Structural Chemistry
AU - Makotchenko, E V
AU - Bykova, E A
AU - Semitut, E Yu
AU - Shubin, Yu. V.
AU - Snytnikov, P V
AU - Plyusnin, P E
PY - 2011
DA - 2011/10/01
PB - Pleiades Publishing
SP - 924-929
IS - 5
VL - 52
SN - 0022-4766
SN - 1573-8779
ER -
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@article{2011_Makotchenko,
author = {E V Makotchenko and E A Bykova and E Yu Semitut and Yu. V. Shubin and P V Snytnikov and P E Plyusnin},
title = {Crystal structure and thermal properties of [Au(en)2]2[Cu(C2O4)2]3·8H2O},
journal = {Journal of Structural Chemistry},
year = {2011},
volume = {52},
publisher = {Pleiades Publishing},
month = {oct},
url = {https://doi.org/10.1134/S002247661105012X},
number = {5},
pages = {924--929},
doi = {10.1134/S002247661105012X}
}
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Makotchenko, E. V., et al. “Crystal structure and thermal properties of [Au(en)2]2[Cu(C2O4)2]3·8H2O.” Journal of Structural Chemistry, vol. 52, no. 5, Oct. 2011, pp. 924-929. https://doi.org/10.1134/S002247661105012X.
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