SYNTHESIS AND STRUCTURE OF A BINUCLEAR Pd(II) CHLORANILATE COMPLEX
Publication type: Journal Article
Publication date: 2021-10-01
scimago Q4
wos Q4
SJR: 0.211
CiteScore: 1.9
Impact factor: 1.4
ISSN: 00224766, 15738779
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
A binuclear complex of palladium (Et3NH)2[Pd2(ca)2(μ-Cl)2]·2CH3CN is synthesized by ligand-exchange reaction between [PdCl2(PhCN)2] and (Et3NH)2ca (ca2– = chloranilate) taken in a 1:1 molar ratio. Its crystal structure is determined. Chloranilate ca2– dianion is coordinated to Pd(II) as C-donor bidentate ligand. Using cyclic voltammetry (CV) of the complex in CH3CN, non-reversible oxidation at Ea = 1.58 V and quasi-reversible reduction with Eb = –0.80 V and Ea = –0.54 V (relative to Ag/AgCl) is found. The electron structure of the complex is examined.
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Romashev N. F. et al. SYNTHESIS AND STRUCTURE OF A BINUCLEAR Pd(II) CHLORANILATE COMPLEX // Journal of Structural Chemistry. 2021. Vol. 62. No. 10. pp. 1573-1579.
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Romashev N. F., Bakaev I. V., Komlyagina V. I., Fomenko I. S., Laricheva Yu. A., Petrov P. A., Gushchin A. L. SYNTHESIS AND STRUCTURE OF A BINUCLEAR Pd(II) CHLORANILATE COMPLEX // Journal of Structural Chemistry. 2021. Vol. 62. No. 10. pp. 1573-1579.
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TY - JOUR
DO - 10.1134/S0022476621100127
UR - https://link.springer.com/10.1134/S0022476621100127
TI - SYNTHESIS AND STRUCTURE OF A BINUCLEAR Pd(II) CHLORANILATE COMPLEX
T2 - Journal of Structural Chemistry
AU - Romashev, N F
AU - Bakaev, I V
AU - Komlyagina, V I
AU - Fomenko, I S
AU - Laricheva, Yu A
AU - Petrov, P. A.
AU - Gushchin, A L
PY - 2021
DA - 2021/10/01
PB - Pleiades Publishing
SP - 1573-1579
IS - 10
VL - 62
SN - 0022-4766
SN - 1573-8779
ER -
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@article{2021_Romashev,
author = {N F Romashev and I V Bakaev and V I Komlyagina and I S Fomenko and Yu A Laricheva and P. A. Petrov and A L Gushchin},
title = {SYNTHESIS AND STRUCTURE OF A BINUCLEAR Pd(II) CHLORANILATE COMPLEX},
journal = {Journal of Structural Chemistry},
year = {2021},
volume = {62},
publisher = {Pleiades Publishing},
month = {oct},
url = {https://link.springer.com/10.1134/S0022476621100127},
number = {10},
pages = {1573--1579},
doi = {10.1134/S0022476621100127}
}
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Romashev, N. F., et al. “SYNTHESIS AND STRUCTURE OF A BINUCLEAR Pd(II) CHLORANILATE COMPLEX.” Journal of Structural Chemistry, vol. 62, no. 10, Oct. 2021, pp. 1573-1579. https://link.springer.com/10.1134/S0022476621100127.
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