SYNTHESIS AND CRYSTAL STRUCTURE OF THE DIRHODIUM TETRAACETATE-DI(CYCLOHEXYLISOCYANIDE) COMPLEX
Publication type: Journal Article
Publication date: 2021-11-01
scimago Q4
wos Q4
SJR: 0.211
CiteScore: 1.9
Impact factor: 1.4
ISSN: 00224766, 15738779
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Dirhodium acetate di(cyclohexylisocyanide) [Rh2(O2CCH3)4(C≡NCy)2] is prepared by treating Rh2(OAc)4 with cyclohexylisocyanide. The crystal structure of [Rh2(O2CCH3)4(C≡NCy)2] is determined by a single crystal X-ray diffraction (XRD) analysis. The title compound crystallizes in the orthorhombic system (space group Ibam). According to the single crystal XRD analysis data, the Rh atom exhibits a slightly distorted octahedral coordination geometry. The Rh1–Rh1–C1 fragment is almost linear (177.87°); ORhO angles are 88.28°, 88.79°, and 91.25°. In addition, the structure of the title compound is unambiguously confirmed by the aggregation of elemental analysis (C, H, N), ESI+–MS, and IR spectroscopy data.
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Grudova M. V. et al. SYNTHESIS AND CRYSTAL STRUCTURE OF THE DIRHODIUM TETRAACETATE-DI(CYCLOHEXYLISOCYANIDE) COMPLEX // Journal of Structural Chemistry. 2021. Vol. 62. No. 11. pp. 1795-1800.
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Grudova M. V., Kubasov A. S., Tskhovrebov A. G. SYNTHESIS AND CRYSTAL STRUCTURE OF THE DIRHODIUM TETRAACETATE-DI(CYCLOHEXYLISOCYANIDE) COMPLEX // Journal of Structural Chemistry. 2021. Vol. 62. No. 11. pp. 1795-1800.
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TY - JOUR
DO - 10.1134/S0022476621110160
UR - https://doi.org/10.1134/S0022476621110160
TI - SYNTHESIS AND CRYSTAL STRUCTURE OF THE DIRHODIUM TETRAACETATE-DI(CYCLOHEXYLISOCYANIDE) COMPLEX
T2 - Journal of Structural Chemistry
AU - Grudova, M V
AU - Kubasov, A. S.
AU - Tskhovrebov, A G
PY - 2021
DA - 2021/11/01
PB - Pleiades Publishing
SP - 1795-1800
IS - 11
VL - 62
SN - 0022-4766
SN - 1573-8779
ER -
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@article{2021_Grudova,
author = {M V Grudova and A. S. Kubasov and A G Tskhovrebov},
title = {SYNTHESIS AND CRYSTAL STRUCTURE OF THE DIRHODIUM TETRAACETATE-DI(CYCLOHEXYLISOCYANIDE) COMPLEX},
journal = {Journal of Structural Chemistry},
year = {2021},
volume = {62},
publisher = {Pleiades Publishing},
month = {nov},
url = {https://doi.org/10.1134/S0022476621110160},
number = {11},
pages = {1795--1800},
doi = {10.1134/S0022476621110160}
}
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Grudova, M. V., et al. “SYNTHESIS AND CRYSTAL STRUCTURE OF THE DIRHODIUM TETRAACETATE-DI(CYCLOHEXYLISOCYANIDE) COMPLEX.” Journal of Structural Chemistry, vol. 62, no. 11, Nov. 2021, pp. 1795-1800. https://doi.org/10.1134/S0022476621110160.
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