Synthesis and crystal structure of diaquadibenzoatobis(nicotinamide)nickel(II)
T V Koksharova
1
,
G G Sadikov
2
,
A S Antsyshkina
2
,
I. S. Gritsenko
1
,
V S Sergienko
2
,
O A Egorova
3
Publication type: Journal Article
Publication date: 2006-06-23
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
A coordination compound of nickel(II) benzoate with nicotinamide [Ni(C6H5COO)2(L)2(H2O)2] (I) (L is nicotinic acid amide) is synthesized and studied by IR spectroscopy. Its crystal structure is solved by X-ray crystallography. The crystals of compound I are monoclinic: a = 7.152 Å, b = 18.266 Å, c = 10.341 Å, β = 109.24°, V = 1275.4 Å3, Z = 2, space group P21/c. Structural units of a crystal of I are centrosymmetric octahedral complex molecules. The coordination environment of the Ni atom contains two O atoms (Ni-O(1) 2.066(2) Å) and two N atoms (Ni-N(1) 2.091(2) Å) of the monodentate-coordinated benzoate anions and nicotinamide molecules, respectively, as well as two O atoms of the H2O molecules (Ni-O(1w) 2.110(2) Å).
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Koksharova T. V. et al. Synthesis and crystal structure of diaquadibenzoatobis(nicotinamide)nickel(II) // Russian Journal of Inorganic Chemistry. 2006. Vol. 51. No. 6. pp. 895-900.
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Koksharova T. V., Sadikov G. G., Antsyshkina A. S., Gritsenko I. S., Sergienko V. S., Egorova O. A. Synthesis and crystal structure of diaquadibenzoatobis(nicotinamide)nickel(II) // Russian Journal of Inorganic Chemistry. 2006. Vol. 51. No. 6. pp. 895-900.
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RIS
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TY - JOUR
DO - 10.1134/S0036023606060088
UR - https://doi.org/10.1134/S0036023606060088
TI - Synthesis and crystal structure of diaquadibenzoatobis(nicotinamide)nickel(II)
T2 - Russian Journal of Inorganic Chemistry
AU - Koksharova, T V
AU - Sadikov, G G
AU - Antsyshkina, A S
AU - Gritsenko, I. S.
AU - Sergienko, V S
AU - Egorova, O A
PY - 2006
DA - 2006/06/23
PB - Pleiades Publishing
SP - 895-900
IS - 6
VL - 51
SN - 0036-0236
SN - 1531-8613
ER -
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BibTex (up to 50 authors)
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@article{2006_Koksharova,
author = {T V Koksharova and G G Sadikov and A S Antsyshkina and I. S. Gritsenko and V S Sergienko and O A Egorova},
title = {Synthesis and crystal structure of diaquadibenzoatobis(nicotinamide)nickel(II)},
journal = {Russian Journal of Inorganic Chemistry},
year = {2006},
volume = {51},
publisher = {Pleiades Publishing},
month = {jun},
url = {https://doi.org/10.1134/S0036023606060088},
number = {6},
pages = {895--900},
doi = {10.1134/S0036023606060088}
}
Cite this
MLA
Copy
Koksharova, T. V., et al. “Synthesis and crystal structure of diaquadibenzoatobis(nicotinamide)nickel(II).” Russian Journal of Inorganic Chemistry, vol. 51, no. 6, Jun. 2006, pp. 895-900. https://doi.org/10.1134/S0036023606060088.
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