Synthesis and crystal structure of the copper(II) valerate complex with nicotinamide
A S Antsyshkina
1
,
T V Koksharova
2
,
G G Sadikov
1
,
I. S. Gritsenko
2
,
V S Sergienko
1
,
O A Egorova
3
Publication type: Journal Article
Publication date: 2006-06-23
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
AbstractA coordination compound of copper(II) valerate with nicotinamide, [CuL(C4H9COO)2]2 (I), has been synthesized, and its crystal structure has been determined by X-ray crystallography. The crystals of I are triclinic: a = 9.1245(9) Å, b = 9.8572(6) Å, c = 11.0944(9) Å, α = 73.51(1)°, β = 79.917(6)°, γ = 72.161(7)°, Z = 2, space group
$$P\bar 1$$
. In the centrosymmetric binuclear molecule of I, the copper atoms (Cu...Cu′, 2.621 Å) are linked through four bidentate chelating valerate ligands (av., Cu-O 1.969 Å). The coordination polyhedron of the Cu atom is a tetragonal pyramid with the nitrogen atom of the pyridine ring in the apical position at a longer distance (Cu-N, 2.190 Å).
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Antsyshkina A. S. et al. Synthesis and crystal structure of the copper(II) valerate complex with nicotinamide // Russian Journal of Inorganic Chemistry. 2006. Vol. 51. No. 6. pp. 901-907.
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Antsyshkina A. S., Koksharova T. V., Sadikov G. G., Gritsenko I. S., Sergienko V. S., Egorova O. A. Synthesis and crystal structure of the copper(II) valerate complex with nicotinamide // Russian Journal of Inorganic Chemistry. 2006. Vol. 51. No. 6. pp. 901-907.
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RIS
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TY - JOUR
DO - 10.1134/S003602360606009X
UR - https://doi.org/10.1134/S003602360606009X
TI - Synthesis and crystal structure of the copper(II) valerate complex with nicotinamide
T2 - Russian Journal of Inorganic Chemistry
AU - Antsyshkina, A S
AU - Koksharova, T V
AU - Sadikov, G G
AU - Gritsenko, I. S.
AU - Sergienko, V S
AU - Egorova, O A
PY - 2006
DA - 2006/06/23
PB - Pleiades Publishing
SP - 901-907
IS - 6
VL - 51
SN - 0036-0236
SN - 1531-8613
ER -
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BibTex (up to 50 authors)
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@article{2006_Antsyshkina,
author = {A S Antsyshkina and T V Koksharova and G G Sadikov and I. S. Gritsenko and V S Sergienko and O A Egorova},
title = {Synthesis and crystal structure of the copper(II) valerate complex with nicotinamide},
journal = {Russian Journal of Inorganic Chemistry},
year = {2006},
volume = {51},
publisher = {Pleiades Publishing},
month = {jun},
url = {https://doi.org/10.1134/S003602360606009X},
number = {6},
pages = {901--907},
doi = {10.1134/S003602360606009X}
}
Cite this
MLA
Copy
Antsyshkina, A. S., et al. “Synthesis and crystal structure of the copper(II) valerate complex with nicotinamide.” Russian Journal of Inorganic Chemistry, vol. 51, no. 6, Jun. 2006, pp. 901-907. https://doi.org/10.1134/S003602360606009X.
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