Synthesis and crystal structure of divaleratobis(nicotinamide)copper(II)
Publication type: Journal Article
Publication date: 2006-10-23
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
A copper(II) valerate complex with nicotinamide (L) [CuL2(C4H9COO)2] (I) has been synthesized and studied by IR spectroscopy and thermogravimetry. The crystal structure has been determined. The crystals of 1 are monoclinic, a = 11.297(1) Å, b = 6.666(1) Å, c = 16.873(2) Å, b = 108.50(1)°, V = 1204.9(3) Å3, Z = 2, space group P21/c. The structural units of the crystal of I are centrosymmetric tetragonal bipyramidal (4+2) complex molecules. The equatorial positions of the bipyramid are occupied by trans-arranged pairs of O (Cu-O, 1.973 Å) and N (Cu-N, 2.006 Å) atoms, and the axial positions are occupied by the second O atoms of the valerate anions located at longer distances (Cu-O, 2.506 Å). The supramolecular associates formed in the crystal are layers of hydrogen-bonded complexes. The disordered hydrocarbon “tails” of the valerate groups point toward the interlayer space.
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Antsyshkina A. S. et al. Synthesis and crystal structure of divaleratobis(nicotinamide)copper(II) // Russian Journal of Inorganic Chemistry. 2006. Vol. 51. No. 10. pp. 1571-1576.
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Antsyshkina A. S., Sadikov G. G., Koksharova T. V., Gritsenko I. S., Sergienko V. S. Synthesis and crystal structure of divaleratobis(nicotinamide)copper(II) // Russian Journal of Inorganic Chemistry. 2006. Vol. 51. No. 10. pp. 1571-1576.
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TY - JOUR
DO - 10.1134/S003602360610010X
UR - https://doi.org/10.1134/S003602360610010X
TI - Synthesis and crystal structure of divaleratobis(nicotinamide)copper(II)
T2 - Russian Journal of Inorganic Chemistry
AU - Antsyshkina, A S
AU - Sadikov, G G
AU - Koksharova, T V
AU - Gritsenko, I. S.
AU - Sergienko, V S
PY - 2006
DA - 2006/10/23
PB - Pleiades Publishing
SP - 1571-1576
IS - 10
VL - 51
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2006_Antsyshkina,
author = {A S Antsyshkina and G G Sadikov and T V Koksharova and I. S. Gritsenko and V S Sergienko},
title = {Synthesis and crystal structure of divaleratobis(nicotinamide)copper(II)},
journal = {Russian Journal of Inorganic Chemistry},
year = {2006},
volume = {51},
publisher = {Pleiades Publishing},
month = {oct},
url = {https://doi.org/10.1134/S003602360610010X},
number = {10},
pages = {1571--1576},
doi = {10.1134/S003602360610010X}
}
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MLA
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Antsyshkina, A. S., et al. “Synthesis and crystal structure of divaleratobis(nicotinamide)copper(II).” Russian Journal of Inorganic Chemistry, vol. 51, no. 10, Oct. 2006, pp. 1571-1576. https://doi.org/10.1134/S003602360610010X.
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