Synthesis, crystal and molecular structure of tetraaquabis(nicotinamide) cobalt(II) phthalate dihydrate
Publication type: Journal Article
Publication date: 2009-08-10
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
The coordination compound of cobalt(II) with nicotinamide [CoL2(H2O)4][C6H4(COO)2] · 2H2O (I) (where L stands for nicotinamide) was synthesized and characterized by IR spectroscopy, conductometry, and thermogravimetry. The X-ray structure of complex I was determined. Crystals are monoclinic: a = 15.630(2) Å, b = 7.550(2) Å, c = 21.035(4) Å, β = 100.90(5)°, V = 2437.4(4) Å3, Z = 4, space group C2/c. The structural units of complex I are centrosymmetrical cations [CoL2(H2O)4]2+, anions [C6H4(COO)2]2− (lying on axis 2), and molecules of waster of crystallization. Complex cations are packed into layers are alternate with layers containing anions and free H2O molecules. This is a classical case of π-π-staking interactions that lead to the formation of supramolecular layered assemblies.
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Antsyshkina A. S. et al. Synthesis, crystal and molecular structure of tetraaquabis(nicotinamide) cobalt(II) phthalate dihydrate // Russian Journal of Inorganic Chemistry. 2009. Vol. 54. No. 8. pp. 1310-1315.
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Antsyshkina A. S., Sadikov G. G., Koksharova T. V., Gritsenko I. S., Sergienko V. S. Synthesis, crystal and molecular structure of tetraaquabis(nicotinamide) cobalt(II) phthalate dihydrate // Russian Journal of Inorganic Chemistry. 2009. Vol. 54. No. 8. pp. 1310-1315.
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TY - JOUR
DO - 10.1134/S003602360908021X
UR - https://doi.org/10.1134/S003602360908021X
TI - Synthesis, crystal and molecular structure of tetraaquabis(nicotinamide) cobalt(II) phthalate dihydrate
T2 - Russian Journal of Inorganic Chemistry
AU - Antsyshkina, A S
AU - Sadikov, G G
AU - Koksharova, T V
AU - Gritsenko, I. S.
AU - Sergienko, V S
PY - 2009
DA - 2009/08/10
PB - Pleiades Publishing
SP - 1310-1315
IS - 8
VL - 54
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2009_Antsyshkina,
author = {A S Antsyshkina and G G Sadikov and T V Koksharova and I. S. Gritsenko and V S Sergienko},
title = {Synthesis, crystal and molecular structure of tetraaquabis(nicotinamide) cobalt(II) phthalate dihydrate},
journal = {Russian Journal of Inorganic Chemistry},
year = {2009},
volume = {54},
publisher = {Pleiades Publishing},
month = {aug},
url = {https://doi.org/10.1134/S003602360908021X},
number = {8},
pages = {1310--1315},
doi = {10.1134/S003602360908021X}
}
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MLA
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Antsyshkina, A. S., et al. “Synthesis, crystal and molecular structure of tetraaquabis(nicotinamide) cobalt(II) phthalate dihydrate.” Russian Journal of Inorganic Chemistry, vol. 54, no. 8, Aug. 2009, pp. 1310-1315. https://doi.org/10.1134/S003602360908021X.
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