Synthesis and structure of palladium triflates with coordinated 3,5-dimethylpyrazole
Publication type: Journal Article
Publication date: 2012-05-21
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
We discovered that reacting Pd3(μ-OOCMe)3 with two moles of trifluoromethanesulfonic acid (Hotf) and then with four moles of 3,5-dimethylpyrazole (Hdmpz) in acetonitrile and benzene produces, in high yields, [Pd(Hdmpz)4](otf)2 and Pd(Hdmpz)4(HOOCMe)2(otf)2, respectively. Reacting PhenPd(OOCMe)2 with Hotf in MeCN yields PhenPd(NCMe)2(otf)2, where labile acetonitrile molecules are substituted by Hdmpz under mild conditions to form PhenPd(Hdmpz)2(otf)2. The structures of complexes have been solved on the basis of X-ray crystallography data.
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Uvarova M. A., Kushan E. V., Nefedov S. Synthesis and structure of palladium triflates with coordinated 3,5-dimethylpyrazole // Russian Journal of Inorganic Chemistry. 2012. Vol. 57. No. 5. pp. 676-683.
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Uvarova M. A., Kushan E. V., Nefedov S. Synthesis and structure of palladium triflates with coordinated 3,5-dimethylpyrazole // Russian Journal of Inorganic Chemistry. 2012. Vol. 57. No. 5. pp. 676-683.
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TY - JOUR
DO - 10.1134/S0036023612050245
UR - https://doi.org/10.1134/S0036023612050245
TI - Synthesis and structure of palladium triflates with coordinated 3,5-dimethylpyrazole
T2 - Russian Journal of Inorganic Chemistry
AU - Uvarova, M A
AU - Kushan, E V
AU - Nefedov, S.E.
PY - 2012
DA - 2012/05/21
PB - Pleiades Publishing
SP - 676-683
IS - 5
VL - 57
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2012_Uvarova,
author = {M A Uvarova and E V Kushan and S.E. Nefedov},
title = {Synthesis and structure of palladium triflates with coordinated 3,5-dimethylpyrazole},
journal = {Russian Journal of Inorganic Chemistry},
year = {2012},
volume = {57},
publisher = {Pleiades Publishing},
month = {may},
url = {https://doi.org/10.1134/S0036023612050245},
number = {5},
pages = {676--683},
doi = {10.1134/S0036023612050245}
}
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MLA
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Uvarova, M. A., et al. “Synthesis and structure of palladium triflates with coordinated 3,5-dimethylpyrazole.” Russian Journal of Inorganic Chemistry, vol. 57, no. 5, May. 2012, pp. 676-683. https://doi.org/10.1134/S0036023612050245.
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