Iron(II) closo-borate complexes with 1,2,4-triazole derivatives: Spin crossover in the iron(II) closo-borate complexes with tris(pyrazol-1-yl)methane
O G Shakirova
1
,
V A Daletskii
1
,
L G Lavrenova
1, 2
,
S.V Trubina
1
,
S. B. Erenburg
1
,
K Yu Zhizhin
3
,
N T Kuzhetsov
3
Publication type: Journal Article
Publication date: 2013-06-13
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
Methods of synthesis of iron(II) complexes containing cluster closo-borate anions—[Fe(Htrz)3]B10Cl10 (I) (HTrz is 1,2,4-triazole), [Fe(NH2Trz)3]B10Cl10 · 2H2O (II) (NH2Trz is 4-amino-1,2,4-triazole), [Fe{HC(pz)3}2]B10Cl10 (III), [Fe{HC(pz)3}2]B10H10 (IV), and [Fe{HC(pz)3}2]B12H12 · 2H2O (V) (HC(pz)3 is tris(pyrazol-1-yl)methane)—have been developed. The compounds have been studied by the static magnetic susceptibility method (78–500 K) and electronic, IR, and EXAFS spectroscopy. Complexes I and II in the temperature range under consideration remain in the high-spin state. Low-spin complex III shows incomplete spin crossover and decomposes on heating above 440 K. Complexes IV and V are characterized by reversible spin crossover 1 A 1 ⇔ 5 T 2 accompanied by thermochromism (the pink ⇔ white color change). The crossover temperature (T c) for IV and V is 375 and 405 K, respectively.
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Total citations:
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Shakirova O. G. et al. Iron(II) closo-borate complexes with 1,2,4-triazole derivatives: Spin crossover in the iron(II) closo-borate complexes with tris(pyrazol-1-yl)methane // Russian Journal of Inorganic Chemistry. 2013. Vol. 58. No. 6. pp. 650-656.
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Shakirova O. G., Daletskii V. A., Lavrenova L. G., Trubina S., Erenburg S. B., Zhizhin K. Yu., Kuzhetsov N. T. Iron(II) closo-borate complexes with 1,2,4-triazole derivatives: Spin crossover in the iron(II) closo-borate complexes with tris(pyrazol-1-yl)methane // Russian Journal of Inorganic Chemistry. 2013. Vol. 58. No. 6. pp. 650-656.
Cite this
RIS
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TY - JOUR
DO - 10.1134/S0036023613060211
UR - https://doi.org/10.1134/S0036023613060211
TI - Iron(II) closo-borate complexes with 1,2,4-triazole derivatives: Spin crossover in the iron(II) closo-borate complexes with tris(pyrazol-1-yl)methane
T2 - Russian Journal of Inorganic Chemistry
AU - Shakirova, O G
AU - Daletskii, V A
AU - Lavrenova, L G
AU - Trubina, S.V
AU - Erenburg, S. B.
AU - Zhizhin, K Yu
AU - Kuzhetsov, N T
PY - 2013
DA - 2013/06/13
PB - Pleiades Publishing
SP - 650-656
IS - 6
VL - 58
SN - 0036-0236
SN - 1531-8613
ER -
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BibTex (up to 50 authors)
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@article{2013_Shakirova,
author = {O G Shakirova and V A Daletskii and L G Lavrenova and S.V Trubina and S. B. Erenburg and K Yu Zhizhin and N T Kuzhetsov},
title = {Iron(II) closo-borate complexes with 1,2,4-triazole derivatives: Spin crossover in the iron(II) closo-borate complexes with tris(pyrazol-1-yl)methane},
journal = {Russian Journal of Inorganic Chemistry},
year = {2013},
volume = {58},
publisher = {Pleiades Publishing},
month = {jun},
url = {https://doi.org/10.1134/S0036023613060211},
number = {6},
pages = {650--656},
doi = {10.1134/S0036023613060211}
}
Cite this
MLA
Copy
Shakirova, O. G., et al. “Iron(II) closo-borate complexes with 1,2,4-triazole derivatives: Spin crossover in the iron(II) closo-borate complexes with tris(pyrazol-1-yl)methane.” Russian Journal of Inorganic Chemistry, vol. 58, no. 6, Jun. 2013, pp. 650-656. https://doi.org/10.1134/S0036023613060211.
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