Russian Journal of Inorganic Chemistry

, том 59 , издание 12 , страницы 1417-1423

Synthesis, crystal and molecular structure of [Co(L)3](OH)Cl· H3Ssal)·H2O, where L is benzhydrazide and H3Ssal is 5-sulfosalycilic acid

A S Antsyshkina ¹

T V Koksharova ²

V S Sergienko ¹

T V Mandzii ²

G G Sadikov ¹

Скрыть аффилиации авторов Показать аффилиации авторов: 2 аффилиации

Kurnakov institute of General and Inorganic Chemistry, Russian Academy of Sciences, Moscow, Russia |

Mechnikov National University, Odessa, Ukraine |

Тип публикации: Journal Article

Дата публикации: 2014-11-26

Pleiades Publishing

Russian Journal of Inorganic Chemistry

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wos Q4

БС2

SJR: 0.270

CiteScore: 3.0

Impact factor: 1.5

ISSN: 00360236, 15318613

DOI: 10.1134/S0036023614120031

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Inorganic Chemistry

Physical and Theoretical Chemistry

Materials Science (miscellaneous)

Краткое описание

The coordination compound [Co(L)3](OH)Cl(H3Ssal) · H2O (I) (L is benzhydrazide, and H3Ssal is 5-sulfosalycilic acid) has been synthesized and studied by IR spectroscopy and X-ray diffraction. Orange crystals are triclinic: a = 9.948(2) Å, b = 12.288(3) Å, c = 14.710(3) Å, α = 109.39(3)°, β = 95.60(3)°, γ = 110.38(3)°, V = 1668.7(6) Å3, Z = 2, space group $P\bar 1$ Structural units of compound I are complex CoL32+ cations, OH− and Cl− anions, sulfosalycilic acid molecules, and an H2O molecule disordered over two positions and linked to each other by hydrogen bonds. Phenyl rings participate in π-π-stacking interaction with the formation of centrosymmetric dimers.

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Russian Journal of General Chemistry	Russian Journal of General Chemistry, 3, 37.5% Russian Journal of General Chemistry 3 публикации, 37.5%
Russian Journal of Inorganic Chemistry	Russian Journal of Inorganic Chemistry, 2, 25% Russian Journal of Inorganic Chemistry 2 публикации, 25%
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya	Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, 1, 12.5% Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya 1 публикация, 12.5%
Journal of Rare Earths	Journal of Rare Earths, 1, 12.5% Journal of Rare Earths 1 публикация, 12.5%
Acta Crystallographica Section E: Crystallographic Communications	Acta Crystallographica Section E: Crystallographic Communications, 1, 12.5% Acta Crystallographica Section E: Crystallographic Communications 1 публикация, 12.5%
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Chinese Society of Rare Earths	Chinese Society of Rare Earths, 1, 12.5% Chinese Society of Rare Earths 1 публикация, 12.5%
International Union of Crystallography (IUCr)	International Union of Crystallography (IUCr), 1, 12.5% International Union of Crystallography (IUCr) 1 публикация, 12.5%
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Antsyshkina A. S. et al. Synthesis, crystal and molecular structure of [Co(L)3](OH)Cl· H3Ssal)·H2O, where L is benzhydrazide and H3Ssal is 5-sulfosalycilic acid // Russian Journal of Inorganic Chemistry. 2014. Vol. 59. No. 12. pp. 1417-1423.

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Antsyshkina A. S., Koksharova T. V., Sergienko V. S., Mandzii T. V., Sadikov G. G. Synthesis, crystal and molecular structure of [Co(L)3](OH)Cl· H3Ssal)·H2O, where L is benzhydrazide and H3Ssal is 5-sulfosalycilic acid // Russian Journal of Inorganic Chemistry. 2014. Vol. 59. No. 12. pp. 1417-1423.

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TY - JOUR

DO - 10.1134/S0036023614120031

UR - https://doi.org/10.1134/S0036023614120031

TI - Synthesis, crystal and molecular structure of [Co(L)3](OH)Cl· H3Ssal)·H2O, where L is benzhydrazide and H3Ssal is 5-sulfosalycilic acid

T2 - Russian Journal of Inorganic Chemistry

AU - Antsyshkina, A S

AU - Koksharova, T V

AU - Sergienko, V S

AU - Mandzii, T V

AU - Sadikov, G G

PY - 2014

DA - 2014/11/26

PB - Pleiades Publishing

SP - 1417-1423

IS - 12

VL - 59

SN - 0036-0236

SN - 1531-8613

ER -

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@article{2014_Antsyshkina,

author = {A S Antsyshkina and T V Koksharova and V S Sergienko and T V Mandzii and G G Sadikov},

title = {Synthesis, crystal and molecular structure of [Co(L)3](OH)Cl· H3Ssal)·H2O, where L is benzhydrazide and H3Ssal is 5-sulfosalycilic acid},

journal = {Russian Journal of Inorganic Chemistry},

year = {2014},

volume = {59},

publisher = {Pleiades Publishing},

month = {nov},

url = {https://doi.org/10.1134/S0036023614120031},

number = {12},

pages = {1417--1423},

doi = {10.1134/S0036023614120031}

}

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Antsyshkina, A. S., et al. “Synthesis, crystal and molecular structure of [Co(L)3](OH)Cl· H3Ssal)·H2O, where L is benzhydrazide and H3Ssal is 5-sulfosalycilic acid.” Russian Journal of Inorganic Chemistry, vol. 59, no. 12, Nov. 2014, pp. 1417-1423. https://doi.org/10.1134/S0036023614120031.