New method for preparation of sulfanyl derivative of closo-decaborate anion [B10H9SH]2−
A. S. Kubasov
1
,
E Yu Matveev
1, 2
,
I N Polyakova
1
,
G A Razgonyaeva
1
,
K Yu Zhizhin
1, 2
,
N. T. Kuznetsov
1
Publication type: Journal Article
Publication date: 2015-02-17
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
Reactions of undecahydrodecaborate anion [B10H11]− and closo-decaborate anion [B10H10]2− with N,N′-disubstituted thioureas were studied. A new simple method for preparing sulfanyl derivative of closo-decaborate anion [B10H9SH]2− in a good yield was proposed on the basis of these reactions. The prepared substituted [B10H9SH]2− and [2-B10H9SC(NH(C6H5))2] were characterized by IR and NMR (1H, 11B, 13C) spectroscopy and ESI/MS spectrometry. X-ray diffraction study was performed for (n-Bu4N)2[2-B10H9SH].
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Kubasov A. S. et al. New method for preparation of sulfanyl derivative of closo-decaborate anion [B10H9SH]2− // Russian Journal of Inorganic Chemistry. 2015. Vol. 60. No. 2. pp. 198-202.
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Kubasov A. S., Matveev E. Yu., Polyakova I. N., Razgonyaeva G. A., Zhizhin K. Yu., Kuznetsov N. T. New method for preparation of sulfanyl derivative of closo-decaborate anion [B10H9SH]2− // Russian Journal of Inorganic Chemistry. 2015. Vol. 60. No. 2. pp. 198-202.
Cite this
RIS
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TY - JOUR
DO - 10.1134/S0036023615020084
UR - https://doi.org/10.1134/S0036023615020084
TI - New method for preparation of sulfanyl derivative of closo-decaborate anion [B10H9SH]2−
T2 - Russian Journal of Inorganic Chemistry
AU - Kubasov, A. S.
AU - Matveev, E Yu
AU - Polyakova, I N
AU - Razgonyaeva, G A
AU - Zhizhin, K Yu
AU - Kuznetsov, N. T.
PY - 2015
DA - 2015/02/17
PB - Pleiades Publishing
SP - 198-202
IS - 2
VL - 60
SN - 0036-0236
SN - 1531-8613
ER -
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BibTex (up to 50 authors)
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@article{2015_Kubasov,
author = {A. S. Kubasov and E Yu Matveev and I N Polyakova and G A Razgonyaeva and K Yu Zhizhin and N. T. Kuznetsov},
title = {New method for preparation of sulfanyl derivative of closo-decaborate anion [B10H9SH]2−},
journal = {Russian Journal of Inorganic Chemistry},
year = {2015},
volume = {60},
publisher = {Pleiades Publishing},
month = {feb},
url = {https://doi.org/10.1134/S0036023615020084},
number = {2},
pages = {198--202},
doi = {10.1134/S0036023615020084}
}
Cite this
MLA
Copy
Kubasov, A. S., et al. “New method for preparation of sulfanyl derivative of closo-decaborate anion [B10H9SH]2−.” Russian Journal of Inorganic Chemistry, vol. 60, no. 2, Feb. 2015, pp. 198-202. https://doi.org/10.1134/S0036023615020084.