Synthesis and magnetic properties of iron(II) closo-borate complexes with tris(3,5-dimethylpyrazol-1-yl)methane
Тип публикации: Journal Article
Дата публикации: 2015-07-07
scimago Q3
wos Q4
БС2
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Краткое описание
Methods are developed for preparing iron(II) complexes with tris(3,5-dimethylpyrazol-1-yl)methane {HC(3,5-dmpz)3} and closo-borate(2-) ions, namely [Fe{HC(3,5-dmpz)3}2]B10H10 · H2O (I) and [Fe{HC(3,5-dmpz)3}2]B12H12 · H2O (II). These complexes were characterized by static magnetic susceptibility measurements (2–325 K), electronic spectroscopy (diffuse reflectance spectra), and IR spectroscopy. The complexes have a distorted octahedral geometry of the coordination polyhedron; the coordination core is FeN6. μeff(T) studies show low-temperature incomplete spin crossover in complex I and antiferromagnetic exchange coupling among iron(II) unpaired electrons at temperatures below 90 K in complex II. Complex I shows thermochromism; the color transition upon cooling is white ↔ pink.
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Shakirova O. G. et al. Synthesis and magnetic properties of iron(II) closo-borate complexes with tris(3,5-dimethylpyrazol-1-yl)methane // Russian Journal of Inorganic Chemistry. 2015. Vol. 60. No. 7. pp. 786-789.
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Shakirova O. G., Lavrenova L. G., Bogomyakov A. S., Zhizhin K. Yu., Kuznetsov N. T. Synthesis and magnetic properties of iron(II) closo-borate complexes with tris(3,5-dimethylpyrazol-1-yl)methane // Russian Journal of Inorganic Chemistry. 2015. Vol. 60. No. 7. pp. 786-789.
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TY - JOUR
DO - 10.1134/S003602361507013X
UR - https://doi.org/10.1134/S003602361507013X
TI - Synthesis and magnetic properties of iron(II) closo-borate complexes with tris(3,5-dimethylpyrazol-1-yl)methane
T2 - Russian Journal of Inorganic Chemistry
AU - Shakirova, O G
AU - Lavrenova, L G
AU - Bogomyakov, A S
AU - Zhizhin, K Yu
AU - Kuznetsov, N. T.
PY - 2015
DA - 2015/07/07
PB - Pleiades Publishing
SP - 786-789
IS - 7
VL - 60
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2015_Shakirova,
author = {O G Shakirova and L G Lavrenova and A S Bogomyakov and K Yu Zhizhin and N. T. Kuznetsov},
title = {Synthesis and magnetic properties of iron(II) closo-borate complexes with tris(3,5-dimethylpyrazol-1-yl)methane},
journal = {Russian Journal of Inorganic Chemistry},
year = {2015},
volume = {60},
publisher = {Pleiades Publishing},
month = {jul},
url = {https://doi.org/10.1134/S003602361507013X},
number = {7},
pages = {786--789},
doi = {10.1134/S003602361507013X}
}
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MLA
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Shakirova, O. G., et al. “Synthesis and magnetic properties of iron(II) closo-borate complexes with tris(3,5-dimethylpyrazol-1-yl)methane.” Russian Journal of Inorganic Chemistry, vol. 60, no. 7, Jul. 2015, pp. 786-789. https://doi.org/10.1134/S003602361507013X.