Malonatobenzhydrazidediaquacobalt(II) hydrate: Synthesis, crystal and molecular structures
Publication type: Journal Article
Publication date: 2016-04-01
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
The coordination compound [Co(L)(Mal)(H2O)2]H2O (I) (L is benzhydrazide, H2Mal is malonic acid) has been synthesized and studied by IR spectroscopy, thermogravimetry, and X-ray diffraction. Crystals are triclinic, a = 7.610(4) Å, b = 7.854(2) Å, c = 12.751(2) Å, α = 75.12(3)°, β = 88.01(3)°, γ = 80.26(3)°, Z = 2, space group $$P\bar 1$$. The structure is molecular. The Co2+ atom has a distorted octahedral coordination. The Co-O and Co-N bond lengths are 2.031-2.129(4) and 2.157(5) Å, respectively. The endocyclic O1Co1N1 bond angles are 77.3(2)° and 90.0(2)° in the five- and six-membered chelate rings, respectively. Molecules of complex I are linked via a great number of hydrogen bonds. The C…C contacts between phenyl rings additionally strengthen the structure.
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Antsyshkina A. S. et al. Malonatobenzhydrazidediaquacobalt(II) hydrate: Synthesis, crystal and molecular structures // Russian Journal of Inorganic Chemistry. 2016. Vol. 61. No. 4. pp. 434-441.
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Antsyshkina A. S., Koksharova T. V., Sadikov G. G., Sergienko V. S., Mandzii T. V. Malonatobenzhydrazidediaquacobalt(II) hydrate: Synthesis, crystal and molecular structures // Russian Journal of Inorganic Chemistry. 2016. Vol. 61. No. 4. pp. 434-441.
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TY - JOUR
DO - 10.1134/S0036023616040045
UR - https://doi.org/10.1134/S0036023616040045
TI - Malonatobenzhydrazidediaquacobalt(II) hydrate: Synthesis, crystal and molecular structures
T2 - Russian Journal of Inorganic Chemistry
AU - Antsyshkina, A S
AU - Koksharova, T V
AU - Sadikov, G G
AU - Sergienko, V S
AU - Mandzii, T V
PY - 2016
DA - 2016/04/01
PB - Pleiades Publishing
SP - 434-441
IS - 4
VL - 61
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2016_Antsyshkina,
author = {A S Antsyshkina and T V Koksharova and G G Sadikov and V S Sergienko and T V Mandzii},
title = {Malonatobenzhydrazidediaquacobalt(II) hydrate: Synthesis, crystal and molecular structures},
journal = {Russian Journal of Inorganic Chemistry},
year = {2016},
volume = {61},
publisher = {Pleiades Publishing},
month = {apr},
url = {https://doi.org/10.1134/S0036023616040045},
number = {4},
pages = {434--441},
doi = {10.1134/S0036023616040045}
}
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MLA
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Antsyshkina, A. S., et al. “Malonatobenzhydrazidediaquacobalt(II) hydrate: Synthesis, crystal and molecular structures.” Russian Journal of Inorganic Chemistry, vol. 61, no. 4, Apr. 2016, pp. 434-441. https://doi.org/10.1134/S0036023616040045.
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