[Co(solv)6][B10H10] (solv = DMF and DMSO) for low-temperature synthesis of borides
V V Avdeeva
1
,
I N Polyakova
1
,
A. V. Vologzhanina
2
,
L. V. Goeva
1
,
G. A. Buzanov
1
,
N B Generalova
1
,
E. A. Malinina
1
,
K Yu Zhizhin
1
,
N. T. Kuznetsov
1
Publication type: Journal Article
Publication date: 2016-09-01
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
The synthesis and structure of complexes [Co(solv)6][B10H10] (solv = DMF and DMSO) have been reported. Both complexes have been prepared in a high yield by the reaction between cobalt(II) salts and closo-decaborates Cat2[B10H10] in the corresponding solvent. The complexes have been characterized by elemental analysis, IR and UV spectroscopy, X-ray powder diffraction, and X-ray crystallography. The thermal properties of the compounds have been studied in the temperature range 20–600°C under argon. The conditions to form cobalt borides have been determined based on the results of thermal analysis, subsequent annealing of the complexes in various conditions, and analysis of IR spectra of the resulting thermolysis products.
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Total citations:
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GOST
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Avdeeva V. V. et al. [Co(solv)6][B10H10] (solv = DMF and DMSO) for low-temperature synthesis of borides // Russian Journal of Inorganic Chemistry. 2016. Vol. 61. No. 9. pp. 1125-1134.
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Avdeeva V. V., Polyakova I. N., Vologzhanina A. V., Goeva L. V., Buzanov G. A., Generalova N. B., Malinina E. A., Zhizhin K. Yu., Kuznetsov N. T. [Co(solv)6][B10H10] (solv = DMF and DMSO) for low-temperature synthesis of borides // Russian Journal of Inorganic Chemistry. 2016. Vol. 61. No. 9. pp. 1125-1134.
Cite this
RIS
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TY - JOUR
DO - 10.1134/S0036023616090023
UR - https://doi.org/10.1134/S0036023616090023
TI - [Co(solv)6][B10H10] (solv = DMF and DMSO) for low-temperature synthesis of borides
T2 - Russian Journal of Inorganic Chemistry
AU - Avdeeva, V V
AU - Polyakova, I N
AU - Vologzhanina, A. V.
AU - Goeva, L. V.
AU - Buzanov, G. A.
AU - Generalova, N B
AU - Malinina, E. A.
AU - Zhizhin, K Yu
AU - Kuznetsov, N. T.
PY - 2016
DA - 2016/09/01
PB - Pleiades Publishing
SP - 1125-1134
IS - 9
VL - 61
SN - 0036-0236
SN - 1531-8613
ER -
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BibTex (up to 50 authors)
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@article{2016_Avdeeva,
author = {V V Avdeeva and I N Polyakova and A. V. Vologzhanina and L. V. Goeva and G. A. Buzanov and N B Generalova and E. A. Malinina and K Yu Zhizhin and N. T. Kuznetsov},
title = {[Co(solv)6][B10H10] (solv = DMF and DMSO) for low-temperature synthesis of borides},
journal = {Russian Journal of Inorganic Chemistry},
year = {2016},
volume = {61},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://doi.org/10.1134/S0036023616090023},
number = {9},
pages = {1125--1134},
doi = {10.1134/S0036023616090023}
}
Cite this
MLA
Copy
Avdeeva, V. V., et al. “[Co(solv)6][B10H10] (solv = DMF and DMSO) for low-temperature synthesis of borides.” Russian Journal of Inorganic Chemistry, vol. 61, no. 9, Sep. 2016, pp. 1125-1134. https://doi.org/10.1134/S0036023616090023.