A new method for the synthesis of carboxonium derivatives of the closo-decaborate anion [2,6-B10H8(O2CR)]–, where R = CH3, C2H5
I N Klyukin
1
,
A P Zhdanov
1
,
A Yu Bykov
1
,
G A Razgonyaeva
1
,
M S Grigorev
2
,
K Yu Zhizhin
1
,
N. T. Kuznetsov
1
Publication type: Journal Article
Publication date: 2017-11-14
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
A single-stage scheme for the synthesis of carboxonium derivatives of the closo-decaborate anion by the reaction between the [B10H11]– anion and carboxylic acids was proposed. Target compounds were separated and characterized by IR and 1H, 11B, 13C NMR spectroscopy. In addition to the target compounds, closo-decaborate cluster opening products ere formed, and in the reaction between the closo-decaborate anion and acetic acid, a polymeric product was observed. The polymeric product (Ph4P) n [2,6,3,7-B10H6O2CCH3] n was characterized by X-ray diffraction.
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Klyukin I. N. et al. A new method for the synthesis of carboxonium derivatives of the closo-decaborate anion [2,6-B10H8(O2CR)]–, where R = CH3, C2H5 // Russian Journal of Inorganic Chemistry. 2017. Vol. 62. No. 11. pp. 1479-1482.
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Klyukin I. N., Zhdanov A. P., Bykov A. Yu., Razgonyaeva G. A., Grigorev M. S., Zhizhin K. Yu., Kuznetsov N. T. A new method for the synthesis of carboxonium derivatives of the closo-decaborate anion [2,6-B10H8(O2CR)]–, where R = CH3, C2H5 // Russian Journal of Inorganic Chemistry. 2017. Vol. 62. No. 11. pp. 1479-1482.
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RIS
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TY - JOUR
DO - 10.1134/S0036023617110109
UR - https://doi.org/10.1134/S0036023617110109
TI - A new method for the synthesis of carboxonium derivatives of the closo-decaborate anion [2,6-B10H8(O2CR)]–, where R = CH3, C2H5
T2 - Russian Journal of Inorganic Chemistry
AU - Klyukin, I N
AU - Zhdanov, A P
AU - Bykov, A Yu
AU - Razgonyaeva, G A
AU - Grigorev, M S
AU - Zhizhin, K Yu
AU - Kuznetsov, N. T.
PY - 2017
DA - 2017/11/14
PB - Pleiades Publishing
SP - 1479-1482
IS - 11
VL - 62
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2017_Klyukin,
author = {I N Klyukin and A P Zhdanov and A Yu Bykov and G A Razgonyaeva and M S Grigorev and K Yu Zhizhin and N. T. Kuznetsov},
title = {A new method for the synthesis of carboxonium derivatives of the closo-decaborate anion [2,6-B10H8(O2CR)]–, where R = CH3, C2H5},
journal = {Russian Journal of Inorganic Chemistry},
year = {2017},
volume = {62},
publisher = {Pleiades Publishing},
month = {nov},
url = {https://doi.org/10.1134/S0036023617110109},
number = {11},
pages = {1479--1482},
doi = {10.1134/S0036023617110109}
}
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Klyukin, I. N., et al. “A new method for the synthesis of carboxonium derivatives of the closo-decaborate anion [2,6-B10H8(O2CR)]–, where R = CH3, C2H5.” Russian Journal of Inorganic Chemistry, vol. 62, no. 11, Nov. 2017, pp. 1479-1482. https://doi.org/10.1134/S0036023617110109.
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