New Methods for the Synthesis of Alkoxy Derivatives of the closo-Decaborate Anion [2-B10H9(OR)]2–, Where R = C2H5, iso-C3H7, С4H9
I N Klyukin
1
,
V V Voinova
1
,
N A Selivanov
1
,
A P Zhdanov
1
,
K Yu Zhizhin
1
,
N. T. Kuznetsov
1
Тип публикации: Journal Article
Дата публикации: 2018-12-10
scimago Q3
wos Q4
БС2
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Краткое описание
A two-stage scheme was proposed for the synthesis of alkoxy derivatives of the closo-decaborate anion [B10H9(OR)]2–, where R = C2H5, iso-C3H7, C4H9. At the first stage, the oxonium derivatives with the general formula [B10H9(OR2)]– were synthesized by the reaction between the [B10H11]–anion and acyclic ethers. At the second stage, the synthesized oxonium derivatives reacted with hydrazine hydrate to form the alkoxy derivatives with the general formula [B10H9(OR)]2–, where R = C2H5, iso-C3H7, C4H9. This approach appreciably increased the yield of target products and simplified their separation. The alkoxy derivatives were separated and characterized by IR and 1H, 11B, and 13C NMR spectroscopy.
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Klyukin I. N. et al. New Methods for the Synthesis of Alkoxy Derivatives of the closo-Decaborate Anion [2-B10H9(OR)]2–, Where R = C2H5, iso-C3H7, С4H9 // Russian Journal of Inorganic Chemistry. 2018. Vol. 63. No. 12. pp. 1546-1551.
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Klyukin I. N., Voinova V. V., Selivanov N. A., Zhdanov A. P., Zhizhin K. Yu., Kuznetsov N. T. New Methods for the Synthesis of Alkoxy Derivatives of the closo-Decaborate Anion [2-B10H9(OR)]2–, Where R = C2H5, iso-C3H7, С4H9 // Russian Journal of Inorganic Chemistry. 2018. Vol. 63. No. 12. pp. 1546-1551.
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TY - JOUR
DO - 10.1134/S0036023618120112
UR - https://doi.org/10.1134/S0036023618120112
TI - New Methods for the Synthesis of Alkoxy Derivatives of the closo-Decaborate Anion [2-B10H9(OR)]2–, Where R = C2H5, iso-C3H7, С4H9
T2 - Russian Journal of Inorganic Chemistry
AU - Klyukin, I N
AU - Voinova, V V
AU - Selivanov, N A
AU - Zhdanov, A P
AU - Zhizhin, K Yu
AU - Kuznetsov, N. T.
PY - 2018
DA - 2018/12/10
PB - Pleiades Publishing
SP - 1546-1551
IS - 12
VL - 63
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2018_Klyukin,
author = {I N Klyukin and V V Voinova and N A Selivanov and A P Zhdanov and K Yu Zhizhin and N. T. Kuznetsov},
title = {New Methods for the Synthesis of Alkoxy Derivatives of the closo-Decaborate Anion [2-B10H9(OR)]2–, Where R = C2H5, iso-C3H7, С4H9},
journal = {Russian Journal of Inorganic Chemistry},
year = {2018},
volume = {63},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://doi.org/10.1134/S0036023618120112},
number = {12},
pages = {1546--1551},
doi = {10.1134/S0036023618120112}
}
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Klyukin, I. N., et al. “New Methods for the Synthesis of Alkoxy Derivatives of the closo-Decaborate Anion [2-B10H9(OR)]2–, Where R = C2H5, iso-C3H7, С4H9.” Russian Journal of Inorganic Chemistry, vol. 63, no. 12, Dec. 2018, pp. 1546-1551. https://doi.org/10.1134/S0036023618120112.
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