Unexpected Formation of an Alcoholate Bridge in the Coordination Polymer of Adduct Zn(OOCPh)2 [O(H)Me]4 and Bidentate γ,γ'-Bipyridyl
Publication type: Journal Article
Publication date: 2019-08-01
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
The recrystallization of Zn(OOCPh)2[O(H)Me]4 (1) (chloroform diffusion to a methanolic solution, dissolution of the powder in boiling MeCN, and exposure of the methanolic solution at room temperature) is found to be accompanied with the formation of {Zn(µ-OOCPh)3Zn(µ-OOCPh)}n polymer single crystals. The diffusion of an MeOH solution of γ,γ'-bipyridyl to a methanolic solution of 1 (in the ratio 1 : 1) gives rise to the formation of {Zn(µ-dipy)(η2-OOCPh)(OOCPh)}n polymer, and the same reaction in the ratio 2 : 1 under strong dilution gives rise to methanol deprotonation to yield {Zn[(µ-OMe)(µ-OOCPh)Zn(OOCPh)]2(µ-dipy)2}n. The product compounds are characterized by chemical analysis, X-ray crystallography, and IR spectroscopy.
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Grineva A. A. et al. Unexpected Formation of an Alcoholate Bridge in the Coordination Polymer of Adduct Zn(OOCPh)2[O(H)Me]4 and Bidentate γ,γ'-Bipyridyl // Russian Journal of Inorganic Chemistry. 2019. Vol. 64. No. 8. pp. 1014-1024.
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Grineva A. A., Grekhova O. D., Datchuk R. R., Uvarova M. A., Nefedov S. Unexpected Formation of an Alcoholate Bridge in the Coordination Polymer of Adduct Zn(OOCPh)2[O(H)Me]4 and Bidentate γ,γ'-Bipyridyl // Russian Journal of Inorganic Chemistry. 2019. Vol. 64. No. 8. pp. 1014-1024.
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TY - JOUR
DO - 10.1134/S0036023619080047
UR - https://doi.org/10.1134/S0036023619080047
TI - Unexpected Formation of an Alcoholate Bridge in the Coordination Polymer of Adduct Zn(OOCPh)2[O(H)Me]4 and Bidentate γ,γ'-Bipyridyl
T2 - Russian Journal of Inorganic Chemistry
AU - Grineva, A A
AU - Grekhova, O D
AU - Datchuk, R R
AU - Uvarova, M A
AU - Nefedov, S.E.
PY - 2019
DA - 2019/08/01
PB - Pleiades Publishing
SP - 1014-1024
IS - 8
VL - 64
SN - 0036-0236
SN - 1531-8613
ER -
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BibTex (up to 50 authors)
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@article{2019_Grineva,
author = {A A Grineva and O D Grekhova and R R Datchuk and M A Uvarova and S.E. Nefedov},
title = {Unexpected Formation of an Alcoholate Bridge in the Coordination Polymer of Adduct Zn(OOCPh)2[O(H)Me]4 and Bidentate γ,γ'-Bipyridyl},
journal = {Russian Journal of Inorganic Chemistry},
year = {2019},
volume = {64},
publisher = {Pleiades Publishing},
month = {aug},
url = {https://doi.org/10.1134/S0036023619080047},
number = {8},
pages = {1014--1024},
doi = {10.1134/S0036023619080047}
}
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MLA
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Grineva, A. A., et al. “Unexpected Formation of an Alcoholate Bridge in the Coordination Polymer of Adduct Zn(OOCPh)2[O(H)Me]4 and Bidentate γ,γ'-Bipyridyl.” Russian Journal of Inorganic Chemistry, vol. 64, no. 8, Aug. 2019, pp. 1014-1024. https://doi.org/10.1134/S0036023619080047.
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