Synthesis and Physicochemical Properties of C-Borylated Esters and Amides Based on the closo-Dodecaborate Anion
Publication type: Journal Article
Publication date: 2020-11-17
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
The nucleophilic addition of the monocarbonyl derivative of the closo-dodecaborate anion [B12H11CO]– with N- and O-nucleophiles has been studied. This process proceeds under mild conditions in high yield. Not only primary and secondary amines but also tertiary ones can be added. The resulting borylated derivatives are thermally unstable, and the C–O and C–N bonds split upon heating forming the initial [B12H11CO]– anion. In an acidic medium in aqueous solutions, borylated derivatives hydrolize forming the carboxylate derivative of general formula [B12H11COOH]–.
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Klyukin I. N. et al. Synthesis and Physicochemical Properties of C-Borylated Esters and Amides Based on the closo-Dodecaborate Anion // Russian Journal of Inorganic Chemistry. 2020. Vol. 65. No. 11. pp. 1637-1641.
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Klyukin I. N., Selivanov N. A., Bykov A. Yu., Zhdanov A. P., Zhizhin K. Yu., Kuznetsov N. T. Synthesis and Physicochemical Properties of C-Borylated Esters and Amides Based on the closo-Dodecaborate Anion // Russian Journal of Inorganic Chemistry. 2020. Vol. 65. No. 11. pp. 1637-1641.
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TY - JOUR
DO - 10.1134/S0036023620110091
UR - https://doi.org/10.1134/S0036023620110091
TI - Synthesis and Physicochemical Properties of C-Borylated Esters and Amides Based on the closo-Dodecaborate Anion
T2 - Russian Journal of Inorganic Chemistry
AU - Klyukin, I N
AU - Selivanov, N A
AU - Bykov, A Yu
AU - Zhdanov, A P
AU - Zhizhin, K Yu
AU - Kuznetsov, N. T.
PY - 2020
DA - 2020/11/17
PB - Pleiades Publishing
SP - 1637-1641
IS - 11
VL - 65
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2020_Klyukin,
author = {I N Klyukin and N A Selivanov and A Yu Bykov and A P Zhdanov and K Yu Zhizhin and N. T. Kuznetsov},
title = {Synthesis and Physicochemical Properties of C-Borylated Esters and Amides Based on the closo-Dodecaborate Anion},
journal = {Russian Journal of Inorganic Chemistry},
year = {2020},
volume = {65},
publisher = {Pleiades Publishing},
month = {nov},
url = {https://doi.org/10.1134/S0036023620110091},
number = {11},
pages = {1637--1641},
doi = {10.1134/S0036023620110091}
}
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Klyukin, I. N., et al. “Synthesis and Physicochemical Properties of C-Borylated Esters and Amides Based on the closo-Dodecaborate Anion.” Russian Journal of Inorganic Chemistry, vol. 65, no. 11, Nov. 2020, pp. 1637-1641. https://doi.org/10.1134/S0036023620110091.
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