Russian Journal of Inorganic Chemistry

, том 67 , издание 7 , страницы 935-939

Synthesis and Crystal Structure of New Oxochloride (Mn,Mg)8Cl3O10

K A Dosaev ¹

S.Ya. Istomin ¹

E. V. ANTIPOV ¹

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Moscow State University, Moscow, Russia |

Тип публикации: Journal Article

Дата публикации: 2022-07-19

Pleiades Publishing

Russian Journal of Inorganic Chemistry

scimago Q3

wos Q4

БС2

SJR: 0.270

CiteScore: 3.0

Impact factor: 1.5

ISSN: 00360236, 15318613

DOI: 10.1134/S0036023622070063

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Inorganic Chemistry

Physical and Theoretical Chemistry

Materials Science (miscellaneous)

Краткое описание

A method has been developed for synthesis of Mn8Cl3O10 oxochloride in an Ar flow (600°C, 8 h) from MnCl2 and MnO2. Some of the Mn2+ cations in this compound have been replaced by Mg2+ cations to fit the Mg0.6Mn7.4Cl3O10 formula. The composition of the oxochloride has been determined from the results of Rietveld refinement of its crystal structure using X-ray powder diffraction data and confirmed by X-ray electron probe analysis. It has been found that the Mg2+ cations in the structure preferentially occupy positions in a cubic array of oxygen atoms (MO8) rather than octahedral MCl6 sites.

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Chemistry of Materials	Chemistry of Materials, 1, 100% Chemistry of Materials 1 публикация, 100%
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Dosaev K. A. et al. Synthesis and Crystal Structure of New Oxochloride (Mn,Mg)8Cl3O10 // Russian Journal of Inorganic Chemistry. 2022. Vol. 67. No. 7. pp. 935-939.

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Dosaev K. A., Istomin S., ANTIPOV E. V. Synthesis and Crystal Structure of New Oxochloride (Mn,Mg)8Cl3O10 // Russian Journal of Inorganic Chemistry. 2022. Vol. 67. No. 7. pp. 935-939.

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TY - JOUR

DO - 10.1134/S0036023622070063

UR - https://link.springer.com/10.1134/S0036023622070063

TI - Synthesis and Crystal Structure of New Oxochloride (Mn,Mg)8Cl3O10

T2 - Russian Journal of Inorganic Chemistry

AU - Dosaev, K A

AU - Istomin, S.Ya.

AU - ANTIPOV, E. V.

PY - 2022

DA - 2022/07/19

PB - Pleiades Publishing

SP - 935-939

IS - 7

VL - 67

SN - 0036-0236

SN - 1531-8613

ER -

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@article{2022_Dosaev,

author = {K A Dosaev and S.Ya. Istomin and E. V. ANTIPOV},

title = {Synthesis and Crystal Structure of New Oxochloride (Mn,Mg)8Cl3O10},

journal = {Russian Journal of Inorganic Chemistry},

year = {2022},

volume = {67},

publisher = {Pleiades Publishing},

month = {jul},

url = {https://link.springer.com/10.1134/S0036023622070063},

number = {7},

pages = {935--939},

doi = {10.1134/S0036023622070063}

}

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Dosaev, K. A., et al. “Synthesis and Crystal Structure of New Oxochloride (Mn,Mg)8Cl3O10.” Russian Journal of Inorganic Chemistry, vol. 67, no. 7, Jul. 2022, pp. 935-939. https://link.springer.com/10.1134/S0036023622070063.