Preconcentration of tetracycline antibiotics on a hyper-crosslinked polystyrene and their determination in waters by high-performance liquid chromatography
Publication type: Journal Article
Publication date: 2015-03-05
scimago Q3
wos Q4
SJR: 0.252
CiteScore: 1.9
Impact factor: 1.1
ISSN: 10619348, 16083199
Analytical Chemistry
Abstract
The possibility of using hyper-crosslinked polystyrene for the dynamic sorption preconcentration (solid-phase extraction) of tetracycline antibiotics (tetracycline, oxytetracycline, chlortetracycline, and doxycycline) from aqueous solutions has been studied. The conditions of the preconcentration of tetracyclines on a microcolumn filled with hyper-crosslinked polystyrene have been optimized. The compounds were desorbed with 2 mL of an acetonitrile-methanol mixture and determined in the eluate by reversed-phase HPLC with an amperometric detector. With preconcentration the limits of detection for tetracyclines were reduced by 90–100 times. The limits of detection were 0.6 ng/mL for oxytetracycline and tetracycline, 1 ng/mL for chlortetracycline, and 2 ng/mL for doxycycline. The method has been used for the analysis of model mixture based on river water.
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Total citations:
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Citations from 2025:
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(12.5%)
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GOST
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Udalova A. Yu. et al. Preconcentration of tetracycline antibiotics on a hyper-crosslinked polystyrene and their determination in waters by high-performance liquid chromatography // Journal of Analytical Chemistry. 2015. Vol. 70. No. 3. pp. 292-297.
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Udalova A. Yu., Dmitrienko S. G., Natchuk S. V., Apyari V. V., Zolotov Y. Preconcentration of tetracycline antibiotics on a hyper-crosslinked polystyrene and their determination in waters by high-performance liquid chromatography // Journal of Analytical Chemistry. 2015. Vol. 70. No. 3. pp. 292-297.
Cite this
RIS
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TY - JOUR
DO - 10.1134/S1061934815030211
UR - http://link.springer.com/10.1134/S1061934815030211
TI - Preconcentration of tetracycline antibiotics on a hyper-crosslinked polystyrene and their determination in waters by high-performance liquid chromatography
T2 - Journal of Analytical Chemistry
AU - Udalova, A Yu
AU - Dmitrienko, S G
AU - Natchuk, S V
AU - Apyari, V V
AU - Zolotov, Yu.A
PY - 2015
DA - 2015/03/05
PB - Pleiades Publishing
SP - 292-297
IS - 3
VL - 70
SN - 1061-9348
SN - 1608-3199
ER -
Cite this
BibTex (up to 50 authors)
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@article{2015_Udalova,
author = {A Yu Udalova and S G Dmitrienko and S V Natchuk and V V Apyari and Yu.A Zolotov},
title = {Preconcentration of tetracycline antibiotics on a hyper-crosslinked polystyrene and their determination in waters by high-performance liquid chromatography},
journal = {Journal of Analytical Chemistry},
year = {2015},
volume = {70},
publisher = {Pleiades Publishing},
month = {mar},
url = {http://link.springer.com/10.1134/S1061934815030211},
number = {3},
pages = {292--297},
doi = {10.1134/S1061934815030211}
}
Cite this
MLA
Copy
Udalova, A. Yu., et al. “Preconcentration of tetracycline antibiotics on a hyper-crosslinked polystyrene and their determination in waters by high-performance liquid chromatography.” Journal of Analytical Chemistry, vol. 70, no. 3, Mar. 2015, pp. 292-297. http://link.springer.com/10.1134/S1061934815030211.