Journal of Analytical Chemistry

, том 70 , издание 11 , страницы 1313-1321

A polymeric magnetic adsorbent based on Fe3O4 nanoparticles and hypercrosslinked polystyrene for the preconcentration of tetracycline antibiotics

V.V. Tolmacheva ¹

V V Apyari ¹

B N Ibragimova ¹

E V Kochuk ¹

S G Dmitrienko ¹

Yu.A Zolotov ¹

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Faculty of Chemistry, Moscow State University, Moscow, Russia |

Тип публикации: Journal Article

Дата публикации: 2015-10-23

Pleiades Publishing

Journal of Analytical Chemistry

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SJR: 0.252

CiteScore: 1.9

Impact factor: 1.1

ISSN: 10619348, 16083199

DOI: 10.1134/S1061934815110155

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Analytical Chemistry

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A magnetic adsorbent based on hypercrosslinked polystyrene (HCPS) and Fe3O4 nanoparticles (HCPS–Fe3O4) is synthesized and investigated. The conditions for its preparation are optimized by varying the weight of adsorbent and the concentration of Fe3O4. A comparative evaluation of the adsorption properties of HCPS–Fe3O4, HCPS, and Fe3O4 to tetracyclines is performed. It is shown that the magnetic adsorbent based on HCPS retains adsorptive properties towards tetracyclines and is easily separated from a solution by applying a magnetic field. The quantitative desorption of tetracyclines is achieved using 4 mL of an acetonitrile–methanol (1: 1) mixture.

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Фурлетов Алексей

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Московский государственный университет имени М.В. Ломоносова

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Tolmacheva V. et al. A polymeric magnetic adsorbent based on Fe3O4 nanoparticles and hypercrosslinked polystyrene for the preconcentration of tetracycline antibiotics // Journal of Analytical Chemistry. 2015. Vol. 70. No. 11. pp. 1313-1321.

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Tolmacheva V., Apyari V. V., Ibragimova B. N., Kochuk E. V., Dmitrienko S. G., Zolotov Y. A polymeric magnetic adsorbent based on Fe3O4 nanoparticles and hypercrosslinked polystyrene for the preconcentration of tetracycline antibiotics // Journal of Analytical Chemistry. 2015. Vol. 70. No. 11. pp. 1313-1321.

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TY - JOUR

DO - 10.1134/S1061934815110155

UR - http://link.springer.com/10.1134/S1061934815110155

TI - A polymeric magnetic adsorbent based on Fe3O4 nanoparticles and hypercrosslinked polystyrene for the preconcentration of tetracycline antibiotics

T2 - Journal of Analytical Chemistry

AU - Tolmacheva, V.V.

AU - Apyari, V V

AU - Ibragimova, B N

AU - Kochuk, E V

AU - Dmitrienko, S G

AU - Zolotov, Yu.A

PY - 2015

DA - 2015/10/23

PB - Pleiades Publishing

SP - 1313-1321

IS - 11

VL - 70

SN - 1061-9348

SN - 1608-3199

ER -

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@article{2015_Tolmacheva,

author = {V.V. Tolmacheva and V V Apyari and B N Ibragimova and E V Kochuk and S G Dmitrienko and Yu.A Zolotov},

title = {A polymeric magnetic adsorbent based on Fe3O4 nanoparticles and hypercrosslinked polystyrene for the preconcentration of tetracycline antibiotics},

journal = {Journal of Analytical Chemistry},

year = {2015},

volume = {70},

publisher = {Pleiades Publishing},

month = {oct},

url = {http://link.springer.com/10.1134/S1061934815110155},

number = {11},

pages = {1313--1321},

doi = {10.1134/S1061934815110155}

}

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Tolmacheva, V.V., et al. “A polymeric magnetic adsorbent based on Fe3O4 nanoparticles and hypercrosslinked polystyrene for the preconcentration of tetracycline antibiotics.” Journal of Analytical Chemistry, vol. 70, no. 11, Oct. 2015, pp. 1313-1321. http://link.springer.com/10.1134/S1061934815110155.